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For previous studies of Jatropha gossypiifolia see: (a) Kupchan, S. M.; Sigel, C. W.; Matz, M. J.; Saenz Renauld, J. A.; Haltiwanger, R. C.; Bryan, R. F. J. Am. Chem. Soc. 1970, 92, 4476. (b) Kupchan, S. M.; Sigel, C. W.; Matz, M. J.; Gilmore, C. J.; Bryan, R. F. J. Am. Chem. Soc. 1976, 98, 2295.
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Taylor, M. D.; Smith, III, A. B.; Furst, G. T.; Gunasekara, S. R.; Bevelle, C. A.; Cordell, G. A.; Kupchan, S. M.; Uchida, H.; Branfman, A. R.; Dailey, Jr., R. G.; Sneden, A. T. J. Am. Chem. Soc. 1983, 105, 3177. For previous studies of Jatropha gossypiifolia see: (a) Kupchan, S. M.; Sigel, C. W.; Matz, M. J.; Saenz Renauld, J. A.; Haltiwanger, R. C.; Bryan, R. F. J. Am. Chem. Soc. 1970, 92, 4476. (b) Kupchan, S. M.; Sigel, C. W.; Matz, M. J.; Gilmore, C. J.; Bryan, R. F. J. Am. Chem. Soc. 1976, 98, 2295.
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Lindberg, T., Ed.; Academic: Orlando, FL (b) Smith, III, A. B.; Guaciaro, M. A.; Schow, S. R.; Wovkulich, P. M.; Toder, B. H.; Hall, T. W. J. Am. Chem. Soc. 1981, 103, 219. See also: Smith, III, A. B.; Guaciaro, M. A.; Schow, S. R.; Wovkulich, P. M.; Toder, B. H.; Hall, T. W. J. Am. Chem. Soc. 1981, 103, 4652. Taylor, M. D.; Smith, III, A. B.; Malamas, M. S. J. Org. Chem. 1983, 48, 4257
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(a) Smith, II I.A.B. Strategies and Tactics in Organic Synthesis; Lindberg, T., Ed.; Academic: Orlando, FL, 1984; Vol. 1, p 223, (b) Smith, III, A. B.; Guaciaro, M. A.; Schow, S. R.; Wovkulich, P. M.; Toder, B. H.; Hall, T. W. J. Am. Chem. Soc. 1981, 103, 219. See also: Smith, III, A. B.; Guaciaro, M. A.; Schow, S. R.; Wovkulich, P. M.; Toder, B. H.; Hall, T. W. J. Am. Chem. Soc. 1981, 103, 4652. Taylor, M. D.; Smith, III, A. B.; Malamas, M. S. J. Org. Chem. 1983, 48, 4257.
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(b) Smith, III, A. B.; Liverton, N. J.; Hrib, N. J.; Sivaramakrishnan, H.; Winzenberg, K. J. Am. Chem. Soc. 1986, 108, 3040.
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(a) Smith, II I.A.B.; Liverton, N. J.; Hrib, N. J.; Sivaramakrishnan, H.; Winzenberg, K. J. Org. Chem. 1985, 50, 3239. (b) Smith, III, A. B.; Liverton, N. J.; Hrib, N. J.; Sivaramakrishnan, H.; Winzenberg, K. J. Am. Chem. Soc. 1986, 108, 3040.
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(b) Banno, K.; Mukaiyama, T. Chem. Lett. 1975, 741. (c) Mukaiyama, T.; Ishida, A. Chem. Lett. 1975, 305.
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(a) Mukaiyama, T.; Yayashi, M. Chem. Lett. 1974, 15. (b) Banno, K.; Mukaiyama, T. Chem. Lett. 1975, 741. (c) Mukaiyama, T.; Ishida, A. Chem. Lett. 1975, 305.
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For the preparation of 12 from the corresponding acid see For (S)-(+)-O-methylmandelic acid see: Bonner, W. A. J. Am. Chem. Soc. 1951, 73, 3126.
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For the preparation of 12 from the corresponding acid see: Jennison, C. P. R.; Mackay, D. Tetrahedron 1973, 29, 1255. For (S)-(+)-O-methylmandelic acid see: Bonner, W. A. J. Am. Chem. Soc. 1951, 73, 3126.
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For the preparation of aluminum hydride from lithium aluminum hydride and 100% sulfuric acid see: (a) (b) Brown, H. C.; Yoon, N. M. J. Am. Chem. Soc. 1966, 88, 1464.
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For the preparation of aluminum hydride from lithium aluminum hydride and 100% sulfuric acid see: (a) Ashby, E. C.; Sanders, J. R.; Claudy, P.; Schwartz, R. J. Am. Chem. Soc. 1973, 95, 6485. (b) Brown, H. C.; Yoon, N. M. J. Am. Chem. Soc. 1966, 88, 1464.
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Wiley: New York See also: Hutchins, R. O.; Hutchins, M. G. K. The Chemistry of Triple-bonded Functional Groups, Patai, S., Rappoport, Z., Eds.; Wiley: Chichester, 1983; Suppl. C, Part 1; p 571, and references therein.
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Fieser, L.; Fieser, M. Reagents for Organic Synthesis, Wiley: New York, 1967; Vol. 1, p 566. See also: Hutchins, R. O.; Hutchins, M. G. K. The Chemistry of Triple-bonded Functional Groups, Patai, S., Rappoport, Z., Eds.; Wiley: Chichester, 1983; Suppl. C, Part 1; p 571, and references therein.
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