A convenient synthesis of exo-brevicomin via a radical C-C bond forming reaction

Synthesis (Germany)

Volumn 1988, Issue 3, 1988, Pages 219-221

  Giese, Bernd ^a   Rupaner, Robert ^a  

^a DARMSTADT UNIVERSITY OF TECHNOLOGY   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

BREVICOMIN;

DRUG ANALYSIS; METHODOLOGY; NONHUMAN; PRELIMINARY COMMUNICATION;

EID: 0023872813     PISSN: 00397881     EISSN: 1437210X     Source Type: Journal    
DOI: 10.1055/s-1988-27517     Document Type: Article

References (24)

1. Silverstein, R. M., Brownless, R. G., Bellas, T. E., Wood, D. L., Browne, L. E. Science 1968, 195, 889.
2. For other syntheses of the enantiomers see: Meyer, H. H. Liebigs Ann. Chem. 1977, 732.
3. Bernardi, R., Fuganti, C., Grasselli, P. Tetrahedron Lett. 1981, 22, 4021.
4. Sherk, A. E., Fraser-Reid, B. J. Org. Chem. 1982, 47, 932.
5. Johnston, B. D., Oehlschlager, A. C. J. Org. Chem. 1982, 47, 5384.
6. Masaki, Y., Nagata, K., Serizawa, Y., Kaji, K. Tetrahedron Lett. 1982, 23, 5553.
7. Asami, M., Mukaiyama, T. Chem. Lett. 1983, 93.
8. Matteson, D. S., Sadhu, K. M. J Am. Chem. Soc. 1983, 105, 2077.
9. Ferrier, R. J., Prasit, P. J. Chem. Soc. Perkin Trans. 1 1983, 1645.
10. Fuganti, C., Grasselli, P., Pedrocchi-Fantoni, G., Servi, S., Zirotti, C. Tetrahedron Lett. 1983, 24, 3753.
11. Wuts, P. G. M., Bigelow, S. S. J. Chem. Soc. Chem. Common. 1984, 736.
12. Larcheveque, M., Laland, J. J. Chem. Soc. Chem. Commun. 1985, 83.
13. Ferrier, R. J., Schmidt, P., Taylor, P. C. J. Chem. Soc. Perkin Trans. 1 1985, 301.
14. Sato, F., Takahashi, O., Kato, T., Kobayashi, Y. J. Chem. Soc. Chem. Commun. 1985, 1638.
15. Hatakeyama, S., Sakurai, K., Takano, S. J. Chem. Soc. Chem. Commun. 1985, 1759.
16. Matteson, D. S., Sadhu, K. M., Peterson, M. L. J. Am. Chem. Soc. 1986, 108, 810.
17. Mori, K., Seu, Y. B. Liehigs Ann. Chem. 1986, 205.
18. Yusufoglu, A., Antons, S., Scharf, H. D. J. Org. Chem. 1986, 51, 3485
19. Hungerbühler, E., Seebach, D. Helv. Chim. Acta 1981, 64, 687, 696.
20. Giese, B. Angew. Chem. 1985, 97, 555;
21. Angew. Chem. Int. Ed. Engl. 1985, 24, 553.
22. Giese, B. Radicals in Organic Synthesis, Pergamon Press, Oxford, 1986.
23. Schurig, V., Wistuba, D., determination of enantiomeric purity by chiral-phase capillary GC.
24. Garegg, P. J. Samuelson, B. J. Chem. Soc. Perkin Trans. 1 1980, 2866.