Use of t-butyldimethylsilylation in the gas chromatographic/mass spectrometric analysis of physiologic compounds found in plasma using electron-impact ionization

Analytical Biochemistry

Volumn 141, Issue 1, 1984, Pages 101-109

  Frederick Schwenk, W ^a,b   Berg, Peter J ^a,b   Beaufrere, Bernard ^a,b   Miles, John M ^a,b   Haymond, Morey W ^a,b  

^a MAYO CLINIC   (United States)

^b MAYO CLINIC COLLEGE OF MEDICINE   (United States)

Author keywords

amino acids; gas chromatography mass spectrometry; glycerol; organic acids; t butyldimethylsilyl derivatives; urea

Indexed keywords

AMINO ACID; FATTY ACID; GLYCEROL; KETONE BODY; LACTIC ACID; LACTIC ACID DERIVATIVE; OXOACID; PYRUVIC ACID DERIVATIVE; SILICON; T BUTYLDIMETHYLSILYL COMPOUNDS; T-BUTYLDIMETHYLSILYL COMPOUNDS; UREA;

ARTICLE; BLOOD; BLOOD ANALYSIS; MASS FRAGMENTOGRAPHY; METHODOLOGY;

AMINO ACIDS; BLOOD CHEMICAL ANALYSIS; FATTY ACIDS, NONESTERIFIED; GLYCEROL; KETO ACIDS; KETONE BODIES; LACTATES; LACTIC ACID; MASS FRAGMENTOGRAPHY; PYRUVATES; SILICON; SUPPORT, NON-U.S. GOV'T; SUPPORT, U.S. GOV'T, P.H.S.; UREA;

EID: 0021763961     PISSN: 00032697     EISSN: 10960309     Source Type: Journal    
DOI: 10.1016/0003-2697(84)90431-7     Document Type: Article

References (16)

1. Gas-liquid chromatography of α-keto acids: Quantification of the branched-chain α-keto acids from physiological sources
2. Determination of ketone body turnover in vivo with stable isotopes, utilizing gas chromatography/mass spectrometry