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Volumn 21, Issue 33, 1980, Pages 3183-3186

A novel synthesis of (±)-trans-chrysanthemic acid

Author keywords

[No Author keywords available]

Indexed keywords

CHRYSANTHEMIC ACID; DRUG ANALYSIS; DRUG IDENTIFICATION; DRUG SYNTHESIS; IN VITRO STUDY; INFRARED SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE; THEORETICAL STUDY;

EID: 0019138704     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(00)77440-5     Document Type: Article
Times cited : (47)

References (28)
  • 8
    • 0018238162 scopus 로고
    • Addition von Organomagnesiumhalogeniden an C  C-Bindungen, XIII. Anlagerungen von Alkylmagnesiumhalogeniden an 3,3-Dimethylcyclopropen; ein neuer Weg zucis- odertrans-Chrysanthemsäure
    • (1978) Justus Liebigs Annalen der Chemie , pp. 1841
    • Lehmkuhl1    Mehler2
  • 13
    • 84918092283 scopus 로고    scopus 로고
    • −1 ; NMR 1.25(s,6H), 1.65(s,6H), 2(s,3H), 5.25(s,2H) is obtained according to 5 with 75 % yield by slow addition (3 h) of acetic anhydride in a methylene chloride solution (1M) of 4a containing diethylamine (excess) and 4-dimethyl-amino pyridine as catalyst (10 %).
  • 16
    • 84918092282 scopus 로고    scopus 로고
    • 3 and quinoleine.
  • 18
    • 84988140497 scopus 로고
    • Catalytic Semihydrogenation of the Triple Bond
    • Catalytic semi-hydrogenation of triple bond
    • (1973) Synthesis , pp. 457
    • Marvell1    Li2
  • 20
    • 84918092281 scopus 로고    scopus 로고
    • 3) : 1.25(s,6H), 1.4(s,6H), 2(OH), 3.45(s,3H), 3.95 (s,1H), 5.75(d,d,J 16 Hz,2H), 7.55(m,3H), 7.75(m,2H) ppm.
  • 21
    • 84918092280 scopus 로고    scopus 로고
    • 3) 1.20(s,6H), 1.2(s,6H), 2(O-H), 3.2(s,1H), 3.5(s,3H), 5.6(d,d,J 16 Hz,2H) ppm.
  • 22
    • 84918092279 scopus 로고    scopus 로고
    • 13C NMR 21.0, 22.25 25.2, 26.6, 26.9, 40.2, 52.25, 78.3, 80.2, 126.5, 128.6, 129, 129.5, 133.3, 134, 134.4, 140.2, 165.8, 169.8 ppm.
  • 23
    • 84918092278 scopus 로고    scopus 로고
    • 3) 27.2, 27.4, 35.2, 47.05, 51.0, 81.2, 128.2, 129, 129.5, 131.3, 132.1, 132.45, 137.30, 165.25, 171.9 ppm.
  • 25
    • 84918092277 scopus 로고    scopus 로고
    • 4) 1.03(s,3H), 1.56(s,3H), 1.73(s,6H), 2.9(d,1H,J 8 Hz), 3.43(s,3H), 5.1(d, broad),1H, 7.6(m,5H) ppm.
  • 26
    • 84918092276 scopus 로고    scopus 로고
    • 4) 1.16(s,3H), 1.61(s,3H), 1.7 (s, broad, 6H), 2.7(d,1H,J 8 Hz), 3.43(s,3H), 5.56(d(broad),1H, 7.6(m,5H) ppm.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.