Technetium Radiopharmaceutical Development. 1. Synthesis, Characterization, and Structure of Dichloro[hydrotris(1-pyrazolyl)borato]oxotechnetium(V)

Journal of the American Chemical Society

Volumn 101, Issue 16, 1979, Pages 4581-4585

  Thomas, Rudy W ^a   Estes, Gregory W ^a   Elder, R C ^a   Deutsch, Edward ^a  

^a UNIVERSITY OF CINCINNATI   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

DRUG ANALYSIS; DRUG STRUCTURE; DRUG SYNTHESIS; IN VITRO STUDY; INFRARED SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE; RAMAN SPECTROMETRY; TECHNETIUM DICHLOROOXOTRIS(PYRAZOL 1 YL)HYDROBORATE; THEORETICAL STUDY; ULTRAVIOLET SPECTROPHOTOMETRY; X RAY ANALYSIS;

EID: 0018701982     PISSN: 00027863     EISSN: 15205126     Source Type: Journal    
DOI: 10.1021/ja00510a024     Document Type: Article

References (44)

1. J.A. Siegel and E. Deutsch, Annu. Rep. Inorg. Gen. Synth., 311 (1976).
2. G. Subramanian, B.A. Rhodes, J.F. Cooper, and V.J. Sodd, Eds., “Radiopharmaceuticals”, The Society of Nuclear Medicine, New York, 1975,
3. J.G. McAfee in “Radiopharmaceuticals”, p 3.
4. N.D. Heindel, H.D. Burns, T. Honda, and L.W. Brady, Eds., “The Chemistry of Radiopharmaceuticals”, Masson Publishing USA, New York, 1978.
5. H.N. Wagner, Jr., “Cardiovascular Nuclear Medicine”, H.W. Strauss, B. Pitt, and A.E. James, Jr., Eds., C.V. Mosby Co., St. Louis, 1974, p 1.
6. “CRC Manual of Nuclear Medicine Procedures”, 2nd ed., J.W. Keyes, Jr., J. Carey, D. Moses, and W. Beierwaltes, Eds., CRC Press, Cleveland, Ohio, 1973.
7. S. Trofimenko, J. Am. Chem. Soc., 89, 3170 (1967).
8. S. Trofimenko, J. Am. Chem. Soc., 91, 588 (1969).
9. S. Trofimenko, J. Am. Chem. Soc., 89, 6288 (1967).
10. S. Trofimenko, Inorg. Chem., 8, 2675 (1969).
11. F.A. Cotton, C.A. Murillo, and B.R. Stults, Inorg. Chim. Acta, 22, 75 (1977).
12. S. Trofimenko, Adv. Chem. Ser., No. 150, 289 (1976).
13. R.C. Elder, L.R. Florian, R.E. Lake, and A.M. Yacynych, Inorg. Chem., 12, 2690 (1973).
14. A. Santoro and A.D. Mighell, Acta Crystallogr., Sect. A. 26, 124 (1976).
15. C.A. Stein, P.E. Ellis, Jr., R.C. Elder, and E.A. Deutsch, Inorg. Chem., 15, 1618 (1976).
16. “International Tables for X-ray Crystallography”, Vol. 4, Kynoch Press, Birmingham, England, 1974 : p 288.
17. D.T. Cromer and J.B. Mann, Acta Crystallogr., Sect. A. 24, 321 (1968).
18. R.F. Stewart, E.R. Davidson, and W.T. Simpson, J. Chem. Phys., 42, 3175 (1965).
19. A. Davison, B.V. DePamphilis, A.G. Jones, and M.A. Davis, J. Am. Chem. Soc., 100, 5570 (1978).
20. J.E. Smith, E.F. Byrne, F.A. Cotton, and J.C. Sekutowski, J. Am. Chem. Soc., 100, 5571 (1978).
21. R.B. King and A. Bond, J. Am. Chem. Soc., 96, 1334 (1974).
22. R.B. King and A. Bond, J. Organomet. Chem., 73, 115 (1974).
23. E.M. Shustorovich, M.A. Porai-Koshits, and Yu. A. Buslaev, Coord. Chem. Rev., 17, 1 (1975).
24. J.E. Fergusson, W. Kirkham, and R.S. Nyholm, “Rhenium”, B.W. Gonser, Ed., American Elsevier, New York, 1962, p 36.
25. A. Earnshaw, B.N. Figgis, J. Lewis, and R.S. Nyholm, Nature (London), 179, 1121 (1957).
26. E. Deutsch, R.C. Elder, B.A. Lange, M.J. Vaal, and D.G. Lay, Proc. Natl. Acad. Sci. U.S.A., 73, 4287 (1976).
27. K. Libson, unpublished results.
28. R.C. Elder, G.W. Estes, and E. Deutsch, Acta Crystallogr., in press.
29. F.A. Cotton and L.W. Shive, Inorg. Chem., 14, 2032 (1975).
30. G. Bandoli, D.A. Clemente, and U. Mazzi, J. Chem. Soc., Dalton Trans., 125 (1976).
31. U. Mazzi, D.A. Clemente, G. Bandoli, L. Magon, and A.A. Orio, Inorg. Chem., 16, 1042 (1977).
32. G. Bandoli, D.A. Clemente, and U. Mazzi, J. Chem. Soc., Dalton Trans., 1837 (1977).
33. F.A. Cotton and L.D. Gage, Nouveau J. Chim., 1, 441 (1977).
34. G. Bandoli, D.A. Clemente, and U. Mazzi, J. Chem. Soc., Dalton Trans., 373 (1978).
35. A.J. Edwards, G.R. Jones, and R.J. Sills, J. Chem. Soc. A. 2521 (1970).
36. B. Krebs, Z. Anorg. Allg. Chem., 380, 146 (1971).
37. F.A. Cotton, B.A. Frenz, and A. Shaver, Inorg. Chim. Acta, 7, 161 (1973).
38. M.R. Churchill, K. Gold, and C.E. Maw Jr., Inorg. Chem., 9, 1597 (1970).
39. B.W. Davies and N.C. Payne, Inorg. Chem., 13, 1843 (1974).
40. R.J. Restivo, G. Ferguson, D.J. O'Sullivan, and F.J. Lalor, Inorg. Chem., 14, 3046 (1975).
41. J.A. McCleverty, D. Seddon, N.A. Bailey, and N.W. Walker, J. Chem. Soc., Dalton Trans., 898 (1976).
42. G. Avitabile, P. Ganis, and M. Nemiroff, Acta Crystallogr., Sect. B. 27, 725
43. E.M. Holt, S.L. Holt, F. Cavalito, and K.J. Watson, Acta Chem. Scand., Ser. A. 30, 225 (1976).
44. M.R. Churchill, B.G. DeBoer, F.J. Rotella, O.M. Abu Salah, and M.I. Bruce, Inorg. Chem., 14, 2051 (1975).