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(a) Compounds 1 crystallize from DMSO to give mononuclear (Y) and carboxylate-bridged dinuclear (La) complexes: Unpublished results.
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15
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0031213456
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6, 25 °C): δ 183.3/151.4/144.8/131.8/121.3/34.8/32.2/24.6/24.0/3.9/-10.8.
-
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-
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17
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0038739775
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note
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3 has been calculated for 2c. Due to severe disorder no solvent molecule, which was identified as hexane by NMR, could be located. Thus, the BYPASS method was applied to account for the disordered solvent contribution to the structure factor in the final refinement.
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0038401604
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note
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2O exhibit bond lengths of 2.475(5)-2.547(5) and 2.398(5)-2.438(5) Å, respectively.
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