Synthesis and trimethylsilyl C-H activation processes of 14-electron Cp*Hf(2 3-dimethyl-1,3-butadiene) trimethylsilylmethyl complexes

Organometallics

Volumn 21, Issue 9, 2002, Pages 1912-1918

  Visser, Cindy ^a   Meetsma, Auke ^a   Hessen, Bart ^a  

^a UNIVERSITY OF GRONINGEN   (Netherlands)

Author keywords

[No Author keywords available]

Indexed keywords

DEPROTONATION;

CHEMICAL BONDS; CRYSTAL STRUCTURE; CRYSTALLIZATION; ELECTRONS; HAFNIUM COMPOUNDS; ISOMERS; ORGANIC SOLVENTS; SYNTHESIS (CHEMICAL); TOLUENE;

ORGANOMETALLICS;

EID: 0013495432     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om011062g     Document Type: Article

References (40)

1. (a) Lappert, M. F.; Pearce, R. J. Chem. Soc., Chem. Commun. 1973, 126.
2. (b) Manriquez, J. M.; Fagan, P. J.; Marks, T. J.; Vollmer, S. H.; Day, C. S.; Day, V. W. J. Am. Chem. Soc. 1979, 101, 5075.
3. (c) Jeske, G.; Lauke, H.; Mauermann, H.; Swepston, P. N.; Schumann, H.; Marks, T. J. J. Am. Chem. Soc. 1985, 107, 8091.
4. (d) Jeske, G.; Schock, L. E.; Swepston, P. N.; Schumann, H.; Marks, T. J. J. Am. Chem. Soc. 1985, 107, 8103.
5. (e) Edelmann, F. T. Metallocenes; Togni, A., Halterman, E. L., Eds.; Wiley-VCH Verlag GmbH: Weinheim, 1998; Vol. 1, Chapter 2, and references therein
6. (f) Anwander, R. Topics in Organometallic Chemistry; Kobayashi, S., Ed.; Springer-Verlag: Berlin, 1999; Vol. 2, Chapter 1, and references therein.
7. (a) Collier, M. R.; Lappert, M. F.; Truelock, M. M. J. Organomet. Chem. 1970, 25, C36.
8. (b) Yagupsky, G.; Mowat, W.; Shortland, A.; Wilkinson, G. J. Chem. Soc., Chem. Commun. 1970, 1369.
9. (c) Davidson, P. J.; Lappert, M. F.; Pearce, R. Acc. Chem. Res. 1974, 7, 209, and references therein.
10. (d) Davidson, P. J.; Lappert, M. F.; Pearce, R. Chem. Rev. 1978, 76, 219, and references therein.
11. (a) Blenkers, J.; De Liefde Meijer, H. J.; Teuben, J. H. Organometallics 1983, 2, 1483.
12. (b) Blenkers, J.; Hessen, B.; van Bolhuis, F.; Wagner, A. J.; Teuben, J. H. Organometallics 1987, 6, 459.
13. (c) Hessen, B.; van Bolhuis, F.; Teuben, J. H. Organometallics 1987, 6, 1352.
14. (d) Ausema, J. B.; Hessen, B.; Teuben, J. H. Recl, Trav. Chim. Pays-Bos 1987, 106, 465.
15. (e) Hessen, B.; Teuben, J. H. Recl. Trav. Chim. Pays-Bas 1988, 107, 208.
16. (f) Hessen, B.; Teuben, J. H. J. Organomet. Chem. 1988, 358, 135.
17. (g) Hessen, B.; Blenkers, J.; Teuben, J. H.; Helgesson, G.; Jagner, S. Organometallics 1989, 8, 830.
18. (h) Hessen, B.; Blenkers, J.; Teuben, J. H.; Helgesson, G.; Jagner, S. Organometallics 1989, 8, 2809.
19. (i) Hessen, B.; van der Hejjden, H. J. Am. Chem. Soc. 1996, 118, 11670.
20. Nakamura, A.; Mashima, K. J. Organomet. Chem. 2001, 621, 224.
21. (a) Thomson, S. K.; Young, G. B. Organometallics 1989, 8, 2068.
22. (b) Tilley, T. D. The Silicon-Heteroatom Bond; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1991; pp 330-331, and references therein.
23. (c) Ankianiec, B. C.; Christou, V.; Hardy, D. T.; Thomson, S. K.; Young G. B. J. Am. Chem. Soc. 1994, 116, 9963.
24. Gielens, E. E. C. G.; Tiesnitsch, J. Y.; Hessen, B.; Teuben, J. H. Organometallics 1998, 17, 1652.
25. (a) Uhl, W. Z. Anorg. Allg. Chem. 1989, 579, 75.
26. (b) Uhl, W.; Koch, M.; Pohl, S.; Saak, W. Z. Anorg. Allg. Chem. 1994, 620, 1619.
27. Wiberg, N.; Wagner, G. Chem. Ber. 1986, 119, 1455.
28. Negishi, E.; Swanson, D. R.; Rousset, C. J. J. Org. Chem. 1990, 55, 5406.
29. (a) Cope, A. C.; Berchtold, G. A.; Ross, D. L. J. Am. Chem. Soc. 1961, 83, 3859.
30. (b) Grummitt, O.; Ardis, A. E.; Fick, J. J. Am. Chem. Soc. 1950, 72, 5167.
31. Blenkers, J. Ph.D. Thesis, 1982, Groningen.
32. Spek, A. L. J. Appl. Crystallogr. 1988, 21, 578.
33. (a) Le Page, Y. J. Appl. Crystallogr. 1987, 20, 264.
34. (b) Le Page, Y. J. Appl. Crystallogr. 1988, 21, 983.
35. Beurskens, P. T.; Beurskens, G.; Gelder, R. de; García-Granda, S.; Gould, R. O.; Israël, R.; Smits, J. M. M. The DIRDIF-99 program system; Crystallography Laboratory: University of Nijmegen, The Netherlands, 1999.
36. Sheldrick, G. M. SHELXL-97, Program for the Refinement of Crystal Structures; University of Göttingen: Germany, 1997.
37. Spek, A. L. PLATON. Program for the Automated Analysis of Molecular Geometry (A Multipurpose Crystallographic Tool); University of Utrecht; The Netherlands, Version of Apr 2001.
38. Meetsma, A. PLUTO, Molecular Graphics Program; University of Groningen: The Netherlands, 2001.
39. (a) Flack, H. D. Acta Crystallogr. 1983, A39, 876-881.
40. (b) Flack, H. D.; Bernardinelli, G. Acta Crystallogr. 1999, A55, 908-915.