Iron carbonyls with bulky thiolate ligands: Crystal structures of [Fe2(CO)6(μ-SC6H2 iPr3 -2,4,6)2] and (C6H2 iPr3 -2,4,6)2S2

Inorganica Chimica Acta

Volumn 284, Issue 1, 1999, Pages 14-19

  Delgado, Esther ^a   Hernández, Elisa ^a   Mansilla, Noelia ^a   Zamora, Félix ^a   Alfonso Martinez Cruz L ^b  

^a UNIVERSIDAD AUTÓNOMA DE MADRID   (Spain)

^b INSTITUTO DE QUÍMICA FÍSICA ROCASOLANO   (Spain)

Author keywords

Carbonyl complexes; Crystal structures; Iron complexes; Thiolate complexes

Indexed keywords

CRYSTAL ATOMIC STRUCTURE; CRYSTAL STRUCTURE; CRYSTALS; PHOSPHORUS COMPOUNDS; SILICON; SULFUR COMPOUNDS; X RAY DIFFRACTION;

CARBONYL COMPLEXES; COMPLEX 1; IRON ATOMS; IRON CARBONYL; IRON COMPLEX; MONONUCLEAR COMPOUNDS; THIOLATE LIGANDS; THIOLATES;

IRON COMPOUNDS;

EID: 0013212963     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/s0020-1693(98)00265-5     Document Type: Article

References (46)

1. W. Lovenberg, Iron-Sulfur Proteins, Academic Press, New York, vols. 1-3, 1973, 1974, 1976.
2. W. Kaim, B. Schwederski, Bioinorganic Chemistry: Inorganic Elements in the Chemistry of Life, Wiley, Chichester, UK, 1994 and references therein.
3. Yeung L.L., Yip Y.Ch., Luh T.-Y. J. Org. Chem. 55:1990;1874.
4. Vicic D.A., Jones W.D. Organometallics. 16:1997;1912.
5. Angelici R.J. Acc. Chem. Res. 21:1988;387.
6. Weigand B.C., Friend C.M. Chem. Rev. 92:1992;491.
7. King R.B., Bisnette M.B. Inorg. Chem. 4:1965;482.
8. J.A. de Beer, R.J. Haines, R. Greatrex, N. Greenwood, J. Chem. Soc. A (1971) 3271.
9. T.E. Burrow, A. Hills, D.L. Hughes, J.D. Lane, R.H. Morris, R.L. Richards, J. Chem. Soc., Dalton Trans. (1991) 1813.
10. T.E. Burrow, D.L. Hughes, A.J. Lough, M.J. Maguire, R.H. Morris, R.L. Richards, J. Chem. Soc., Dalton Trans. (1995) 2583.
11. Bianchini C., Frediani P., Herrera V., Jiménez M.V., Meli A., Rincón L., Sánchez-Delgado R.A., Vizza F. J. Am. Chem. Soc. 117:1995;4333.
12. Kiiski U., Pakkanen T.A., Krause O. J. Mol. Catal. 50:1989;143.
13. Gates B.C., Lamb H.H. J. Mol. Catal. 52:1989;1.
14. Allum K.G., Hancock R.D., Howell I.V., Lester T.E., Mckenzie S., Pitkethly R.C., Robinson P.J. J. Organomet. Chem. 107:1976;393.
15. D.F. Shriver, M.A. Drezdzon, The Manipulation of Air Sensitive Compounds, 2nd ed, Wiley, New York, 1986.
16. D.D. Perrin, W.L.F. Armarego, D.R. Perrin, Purification of Laboratory Chemicals, 2nd ed, Pergamon, Oxford, 1980.
17. P.J. Blower, J.R. Dilworth, J.P. Hutchinson, J.A. Zubieta, J. Chem. Soc., Dalton Trans. (1985) 1533.
18. Kowalski J., Chojnowski J. J. Organomet. Chem. 365:1988;285.
19. King R.B., Stone F.G.A. Inorg. Synth. 7:1963;110.
20. De Beer J.A., Haines R.J. J. Organomet. Chem. 24:1970;757.
21. International Tables for Crystallography, Kluwer, Dordrecht, The Netherlands, vol. C, 1992.
22. Altomare A., Burla M.C., Camalli M., Cascarano G., Giacovazzo C., Guagliardi A., Polidori G. J. Appl. Crystallogr. 27:1994;435.
23. G.M. Sheldrick, Acta Crystallogr., Sect. A 46 (1990) 467.
24. G.M. Sheldrick, (1993), in preparation for J. Appl. Crystallogr., computing-structure-solution SHELXS-86 (Sheldrick, 1990)- computing-structure-refinement SHELXS-93 (Sheldrick, 1993).
25. A.C.T. North, D.C. Phillips, F.S. Mathews, Acta Crystallogr., Sect. A 24 (1968) 351.
26. Kostiner E., Reddy M.L.N., Urch D.S., Massey A.G. J. Organomet. Chem. 15:1968;383.
27. Winter A., Zsolnai L., Huttner G. Chem. Ber. 115:1982;1286.
28. Bor G. J. Organomet. Chem. 94:1975;181.
29. Seyferth D., Henderson R.S., Song L.-Ch. Organometallics. 1:1982;125.
30. Ellgen P.C., Gerlach J.N. Inorg. Chem. 12:1973;2526.
31. Delgado E., Hernández E., Rossell O., Seco M., Gutierrez-Puebla E., Ruiz C. J. Organomet. Chem. 455:1993;177.
32. Maresca L., Greggio F., Brignadello G.S., Bor G. Inorg. Chim. Acta. 5:1971;667.
33. De Beer J.A., Haines R.J. J. Organomet. Chem. 36:1972;297.
34. Ahmad M., Bruce R., Knox G.R. J. Organomet. Chem. 6:1966;1.
35. Treichel P.M., Rublein E.K. J. Organomet. Chem. 423:1992;391.
36. J. Cooke, M. Green, F.G.A. Stone, J. Chem. Soc. (A) (1968) 170.
37. Treichel P.M., Rosenhein L.D., Schmidt M.S. Inorg. Chem. 22:1983;3960.
38. C.K. Johnson, ORTEP, Report ORNL-3794, Oak Ridge National Laboratory, Oak Ridge, TN, 1965.
39. Dahl L.F., Wei C.-H. Inorg. Chem. 2:1963;328.
40. Henslee W., Davis R.E. Cryst. Struct. Comm. 1:1972;403.
41. Le Borgne G., Grandjean D., Mathieu R., Poilblanc R. J. Organomet. Chem. 131:1977;429.
42. Woodard C.M., Brown D.S., Lee J.D., Massey A.G. J. Organomet. Chem. 121:1976;333.
43. S.R. Hall, J.M. Stewart (Eds.), XTAL3.2, (1994), Universities of Western Australia and Maryland, Perth, WA, Australia.
44. J.D. Lee, M.W.R. Bryant, Acta Crystallogr., Sect. B 25 (1969) 2094.
45. Marsch R.E. Acta Crystallogr. 5:1952;458.
46. A. Edelmann, S. Brooker, N. Bertel, M. Noltemeyer, H.W. Roesky, G.M. Sheldrick, F.T. Edelmann, Z. Naturforsch., Teil B 47 (1992) 305.