Crystal structures of neutral trigonal bipyramidal [NiCl2(PMePh2)(PNMe2)] · CH2Cl2 and cationic square planar [NiCl(PMePh2)(PNMe2)][PF6] complexes

Zeitschrift fur Kristallographie - New Crystal Structures

Volumn 212, Issue 10, 1997, Pages 745-751

  Crociani, L ^a   Refosco, F ^a   Tisato, F ^a   Dolmella, A ^b   Gatto, S ^b   Bandoli, G ^b  

^a CNR   (Italy)

^b UNIVERSITY OF PADOVA   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0013156264     PISSN: 14337266     EISSN: None     Source Type: Journal    
DOI: 10.1524/zkri.1997.212.10.745     Document Type: Article

References (21)

1. Anderson, G. K.; Kumar, R.; Platinum(II) complexes of unsymmetrical, potentially bidentate ligands. Inorg. Chem. 23 (1984) 4064-4068.
2. Roundhill, D. M.; Bechtold, R. A.; Roundhill, S. G. N.: Synthetic, structural, stereochemical, and catalytic studies on carbonyliridium(I) complexes. Inorg. Chem. 19 (1980) 284-289; Mudalige, D. C.; Rettig, S. J.; James, B. R.; Cullen, W. R.: Molecular-hydrogen,-nitrogen and monohydride derivatives of a structurally characterised ruthenium(II) complex. J. Chem. Soc. Chem. Commun. (1993) 830-832; Farnetti, E.; Nardin, G.: Graziani, M.: Intramolecular activation of a N-methyl C-H bond by an electron rich iridium centre. J. Chem. Soc. Chem. Commun. (1989) 1264-1265.
3. Braunstein, P.; Pietsch, J.; Chauvin, Y; Mercier, S.; Saussine, L.; DeCian, A.; Fischer, J.: Phenyl nickel complexes with a chelating RN ligand. J. Chem. Soc. Dalton Trans. (1996) 3571-3574.
4. Habtemariam, A.; Sadler, P. J.: Design of chelate ring-opening platinum anticancer complexes: reversible binding to guanine. J. Chem. Soc. Chem. Commun. (1996) 1785-1786.
5. Lutz, E. F.: Shell higher olefins process. J. Chem. Educ. 63 (1986) 202-203.
6. Keim, W.: Nickel: An element with wide application in industrial homogeneus catalysis. Angew. Chem. Int. Ed. Engl. 29 (1990) 235-244.
7. Bonnet, M. C.; Dahan, F.; Ecke, A.; Keim, W.; Schulz, R. P.; Tkatchenko, I.: Synthesis of cationic and neutral methallyl nickel complexes and applications in ethene oligomerisation. J. Chem. Soc. Chem. Commun. (1994) 615-616.
8. Britovsek, G. J. P.; Keim, W.; Mecking, S.; Sainz, D.; Wagner, T.: Hemilabile R O-ligands in palladium catalysed C-C linkages: codimerization of ethylene and styrene and cooligomerization of ethylene and carbon monoxide. J. Chem. Soc. Chem. Commun. (1993) 1632-1634.
9. Allen, E. A.; Wilkinson, W.: The vibrational spectra of some four-coordinate complexes of palladium and nickel with various phosphine ligands. Spectrochim. Acta 30A (1974) 1219-1224.
10. Fritz, H. P.; Gordon, I. R.; Schwarzhans, K. E.; Venanzi, L. M.: Some complexes of palladium(II) and platinum(II) with mixed phosphorus-nitrogen ligands. J. Chem. Soc. (1965) 5210-5216.
11. Sheldrick, G. M.: Program Package SHELXTL-plus. Release 4.1. Siemens Analytical X-Ray Instruments Inc., Madison (WI 53719), USA 1990.
12. Johnson, C. K.: ORTEPII. Report ORNL-5138. Oak Ridge National Laboratory, Tennessee, USA 1976.
13. Motherwell, S.; Clegg, W.: PLUTO. Program for plotting molecular and crystal structures. University of Cambridge, England 1978.
14. Crociani, L.; Refosco, F.; Tisato, F.; Gatto, S.; Corain, B.: Neutral and cationic nickel(II) complexes of phosphino-amines. Inorg. Chim. Acta 249 (1996) 131-133.
15. Orpen, A. G.; Brammer, L.: Allen, F. H.; Kennard, O.; Watson, D. G.; Taylor, R.: Tables of bond lengths determined by X-ray and neutron diffraction. Part 2. Organometallic compounds and co-ordination complexes of the d-and /-block metals. J. Chem. Soc. Dalton Trans. (1989) S1-S83.
16. Allen, F. H.; Bellard, S.; Brice, M. D.; Cartwright, B. A.; Doubleday, A.; Higgs, H.; Hummelink, T.; Hummelink-Peters, B. G.; Kennard, O.; Motherwell, W. D. S.; Rodgers, J. R.; Watson, D. G.: The Cambridge Crystallographic Data Centre: computer-based search, retrieval, analysis and display of information. Acta Crystallogr. B35 (1979) 2331-2339; CSD Database, Release 5.12, October 1996.
17. Curran, R.; Cunningham, J. A.; Eisenberg, R.: The crystal and molecular structure of trans-bis(diphenyl-o-selenolatophenylphosphine) nickel(II). Inorg. Chem. 9 (1970) 2749-2754.
18. Miedaner, A.; Haltiwanger, R. C.; DuBois, D. L.: Relationship between the bite size of diphosphine ligands and tetrahedral distortions of “square-planar” nickel(II) complexes. Inorg. Chem. 30 (1991) 417-427.
19. Di Vaira, M.; Stoppioni, P.: McCleverty, J. A.: Synthesis and characterization of new iron(II), cobalt(II) and nickel(II) complexes with Jt donor acceptor ligands. X-ray structural characterization of [(pp,)Ni(PY)][BF4]2. Gazz. Chim. [tel. 125 (1995) 277-281.
20. Alyea, E. C.; Ferguson, G.; Parvez, M.; Davies, J. E.: Tri-f-butylphosphonium tribromo (tri-r-butylphosphine)nickelate(II). Cryst. Struct. Comm. 11 (1982) 1713-1717.
21. Kyba, E. P.; Davis, R. E.; Liu, S.-T.; Hassett, K. A.; Larson, S. B.: Structural characterization of tridentate 11-membered phosphino macrocyclic complexes of transition metals. Inorg. Chem. 24 (1985) 4629-4634.