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Volumn 23, Issue 43, 1982, Pages 4411-4414

Design and reactivity of organic functional groups: the highly crystalline 2-alkoxy N,N′-diphenyl-1,3,2-diazaphospholanes and their facile conversion into alkyl halides

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Indexed keywords


EID: 0012789169     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(00)85615-4     Document Type: Article
Times cited : (14)

References (18)
  • 9
    • 85077634689 scopus 로고
    • The Use of Diethyl Azodicarboxylate and Triphenylphosphine in Synthesis and Transformation of Natural Products
    • and references cited therein
    • (1981) Synthesis , pp. 1
    • Mitsunobu1
  • 15
    • 84918345767 scopus 로고    scopus 로고
    • Prepared from N,N′-diphenyl-1,2-diaminoethane (5 g, 23.6 moles) and tris(dimethylamino)phosphine ( 3.85 g., 23.6 mmoles) in refluxing toluene (24h). The product crystallizes upon cooling. Recrystallization from toluene gave pure reagent (85%), m.p. 140°;
  • 17
    • 84918345766 scopus 로고    scopus 로고
    • New compounds gave correct microanalyses and satisfactory spectroscopic characteristics.
  • 18
    • 84918345765 scopus 로고    scopus 로고
    • D-12°, identical with an authentic specimen.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.