Preparation, properties, and structures of [IrCl(diphosphine)]2 (diphosphine = (R)-BINAP and BPBP)

Chemistry Letters

Volumn , Issue 12, 1997, Pages 1215-1216

  Yamagata, Tsuneaki ^a   Iseki, Aika ^a   Tani, Kazuhide ^a  

^a OSAKA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0012716226     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1997.1215     Document Type: Article

References (18)

1. See for example: a) K. Tani, J.-I. Onouchi, T. Yamagata, and Y. Kataoka, Chem. Lett., 1995, 955.
2. b) T. Morimoto, N. Suzuki, and K. Achiwa, Heterocycles, 43, 2557 (1996) and references therein.
3. a) P. S. Sheridan and F. Jardine, in "Comprehensive Coordination Chemistry," ed by G. Wilkinson, R. D. Giollard, and J. A. McCleverty, Pergamon Press, Oxford (1987), Vol. 4, pp 912 -913.
4. b) N. Serpone and M. A. Jamieson, in "Comprehensive Coordination Chemistry," ed by G. Wilkinson, R. D. Giollard, and J. A. McCleverty; Pergamon Press, Oxford (1987), Vol. 4, pp 1108-1105.
5. c) A. A. Del Paggio, R. A. Anderson, and E. L. Muetterties, Organometallics, 6, 1260 (1987).
6. R. C. Schnabel and D. M. Roddick, Inorg. Chem., 32, 1513 (1993).
7. J. H. Herde, J. C. Lambert, and C. V. Senoff, Inorg. Synth., 15, 18 (1974).
8. 2, 109.25 MHz, 35°C): δ 13.5(s).
9. a) Preliminary results have been presented at the 72th Spring Annual Meeting of the Chemical Society of Japan, Tokyo, March, 1997, Abstr., 3E238 and OMCOS 9, Göttingen, July, 1997, Abstr., 362.
10. b) Complex a has recently been prepared and characterized independently by A. Togni and co-workers, J. Am. Chem. Soc., in press (A. Togni, ETH, private communication).
11. 3. All calculations were carried out on SGI Power Challenge (Silicon Graphics) workstation at the Research Center for Protein Engineering, Institute for Protein Research, Osaka University. The authors have deposited atomic coordinates at the Cambridge Crystallographic Data Centre. The coordinates can be obtained on the request from the Director, Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 IEZ, UK.
12. A. C. T. North, D. C. Phillips, and F. S. Mathews, Acta Cryst. A24, 351 (1968).
13. G. M. Sheldrick "SHELXS-86. Program for the Solution of Crystal Structures". University of Göttingen, Germany, (1985).
14. S. Karle, Acta Cryst., B24, 182 (1968). teXsan: Single Crystal Structure Analysis Software, Version 1.6f (1994). Molecular Structure Corporation, The Woodlands, TX. 77381.
15. S. Karle, Acta Cryst., B24, 182 (1968). teXsan: Single Crystal Structure Analysis Software, Version 1.6f (1994). Molecular Structure Corporation, The Woodlands, TX. 77381.
16. G. M. Sheldrick, "SHELXL-93. Program for Refinement of Crystal Structure"; University of Göttingen, Göttingen, Germany.
17. 3: C, 66.93; H, 4.26. Found: C, 67.10; H, 4.36.
18. Preliminary results have been presented at 31th International Conference on Coordination Chemistry, Vancouver, Canada, August, 1996, Abstr., 3L9 and International Union of Crystallography, XVII Congress and General Assembly, Seattle, Washington, August, 1996, Abstr., PS 07.00.50.