Synthesis and characterization of 1,1′-diphospharuthenocenes

Organometallics

Volumn 21, Issue 14, 2002, Pages 3062-3065

  Ogasawara, Masamichi ^a   Nagano, Takashi ^a   Yoshida, Kazuhiro ^a   Hayashi, Tamio ^a  

^a KYOTO UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

LIGANDS;

COMPLEXATION; CRYSTAL STRUCTURE; LITHIUM COMPOUNDS; SINGLE CRYSTALS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION ANALYSIS;

ORGANOMETALLICS;

EID: 0012253662     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om020189i     Document Type: Article

References (42)

1. Mathey, F.; Fischer, J.; Nelson, J. H. Struct. Bonding 1983, 55, 153.
2. Mathey, F. New J. Chem. 1987, 11, 585.
3. Mathey, F. J. Organomet. Chem. 1990, 400, 149.
4. Mathey, F. Coord. Chem. Rev. 1994, 137, 1.
5. Mathey, F.; Mitschler, A.; Weiss, R. J. Am. Chem. Soc. 1977, 99, 3537.
6. Mathey, F. J. Organomet. Chem. 1977, 139, 77.
7. de Lauzon, G.; Mathey, F.; Simalty, M. J. Organomet. Chem. 1978, 156, C33.
8. de Lauzon, G.; Deschamps, B.; Fischer, J.; Mathey, F.; Mitschler, A. J. Am. Chem. Soc. 1980, 102, 994.
9. de Lauzon, G.; Deschamps, B.; Mathey, F. Nouv. J. Chim. 1980, 4, 683.
10. For the recent application of phosphaferrocenes to organic synthesis, see: (a) Ganter, C.; Kaulen, C.; Englert, U. Organometallics 1999, 18, 5444.
11. Shintani, R.; Lo, M. M.-C.; Fu, G. C. Org. Lett. 2000, 2, 3695.
12. Tanaka, K.; Qiao, S.; Tobisu, M.; Lo, M. M.-C.; Fu, G. C. J. Am. Chem. Soc. 2000, 122, 9870.
13. Sava, X.; Ricard, L.; Mathey, F.; Le Floch, P. Organometallics 2000, 19, 4899.
14. Ogasawara, M.; Yoshida, K.; Hayashi, T. Organometallics 2001, 20, 3913.
15. Carmichael, D.; Ricard, L.; Mathey, F. J. Chem. Soc., Chem. Commun. 1994, 1167.
16. Herberich, G. E.; Ganter, B. Organometallics 1997, 16, 522.
17. Herberich, G. E.; Ganter, B.; Englert, U. Struct. Chem. 1998, 9, 359.
18. Desmurs, P.; Dormond, A.; Nief, F.; Baudry, D. Bull. Soc. Chim. Fr. 1997, 134, 683.
19. Soberer, O. J.; Brück, T.; Wolmershäuser, G. Chem. Ber. 1988, 121, 927.
20. Hitchcock, P. B.; Matos, R. M.; Nixon, J. F. J. Organomet, Chem. 1993, 462, 319.
21. Hitchcock, P. B.; Nixon, J. F.; Matos, E. M. J. Organomet. Chem. 1995, 490, 155.
22. Rink, B.; Scherer, O. J.; Wolmersha ̈user, G. Chem. Ber. 1995, 128, 71.
23. Hitchcock, P. B.; Johnson, J. A.; Nixon, J. F. Organometallics 1995, 14, 4382.
24. Diphosphastibolyl-Ru(II) complexes are also known. See: (a) Francis, M. D.; Hibbs, D. E.; Hursthouse, M. B.; Jones, C.; Malik, K. M. A. Chem. Commun. 1996, 1591.
25. Black, S. J.; Francis, M. D.; Jones, C. J. Chem. Soc., Dalton Trans. 1997, 2183.
26. Ogasawara, M.; Yoshida, K.; Hayashi, T. Organometallics 2001, 20, 1014.
27. Mathey, F.; de Lauzon, G. Organomet. Synth. 1986, 3, 259.
28. Roberts, R. M. G.; Silver, J.; Wells, A. S. Inorg. Chim. Acta 1986, 119, 1.
29. n in ethanol gave ruthenocene in high yield. See: (a) Liles, D. C.; Shaver, A.; Singleton, E.; Wiege, M. B. J. Organomet. Chem. 1985, 288, C33.
30. Albers, M. O.; Liles, D. C.; Robinson, D. J.; Shaver, A.; Singleton, E.; Wiege, M. B.; Boeyens, J. C. A.; Levendis, D. C. Organometallics 1986, 5, 2321.
31. Hitchcock, P. B.; Lawless, G. A.; Maziano, I. J. Organomet, Chem. 1997, 527, 305.
32. Qiao, S.; Hoic, D. A.; Fu, G. C. Organometallics 1998, 17, 773.
33. Mathey, F. J. Organomet. Chem. 1978, 154, C13.
34. Breque, A.; Mathey, F.; Santini, C. J. Organomet. Chem. 1979, 165, 129.
35. Bourumeau, K.; Gaumont, A.-C.; Denis, J.-M. J. Organomet. Chem. 1997, 529, 205.
36. Zweifel, G.; Lynd, R. A.; Murray, R. E. Synthesis 1977, 52.
37. Breque, A.; Mathey, F.; Savignac, P. Synthesis 1981, 983.
38. Fagan, P. J.; Nugent, W. A.; Calabrese, J. C. J. Am. Chem. Soc. 1994, 116, 1880.
39. Albers, M. O.; Singleton, E.; Yates, Y. E. Inorg. Synth. 1989, 26, 253.
40. Only the data for the phospholyl ring-carbon signals are given.
41. CrystalStructure 2.00, Crystal Structure Analysis Package; Rigaku and MSC, 2001.
42. Watkin, D. J.; Prout, C. K.; Carruthers, J. R.; Betteridge, P. W. CRYSTALS Issue 10; Chemical Crystallography Laboratory: Oxford, UK.