Catalytic hydrogenolysis of aromatic halides with sodium hydride of nanometric size

Chemistry Letters

Volumn , Issue 12, 1996, Pages 1059-1060

  Li, Haiqing ^a   Liao, Shijian ^a   Xu, Yun ^a  

^a DALIAN INSTITUTE OF CHEMICAL PHYSICS   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0011961181     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1996.1059     Document Type: Article

References (16)

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16. 4 were added under argon. The argon was evacuated and hydrogen was passed into the reaction vessel. The uptake of hydrogen was measured with a constant-pressure gas burette. The reaction was maintained at 40°C in an oil bath and the reaction mixture was stirred magnetically. After reaction was completed, a sodium hydride slurry containing Ti species was obtained. The prepared sodium hydride slurry was centrifuged and the solids were washed three times with THF and then evacuated at 60°C to dryness. The NaH* powder was obtained.