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16
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85033749176
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note
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The addition of 7 to 5 at -100°C produced a 15 : 1 mixture of 9 and 10 in 47% yield.
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17
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0007562550
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Kagan, H. B.; Namy, J. L. Tetrahedron 1986, 42, 6573; Imamoto, T. Pure Appl. Chem. 1990, 62, 747.
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Kagan, H.B.1
Namy, J.L.2
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18
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84950086506
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Kagan, H. B.; Namy, J. L. Tetrahedron 1986, 42, 6573; Imamoto, T. Pure Appl. Chem. 1990, 62, 747.
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Imamoto, T.1
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20
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24
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0003463148
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John Wiley & Sons, Inc.
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Greene, T. W.; Wuts, P. G. M. In Protective Groups in Organic Synthesis, 2nd ed.; John Wiley & Sons, Inc., 1991; p88.
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Greene, T.W.1
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25
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85033746762
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note
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Under basic conditions (TMSOTf and hexamethyldisilazane), only TMS group could be introduced to 17. However, the reductive elimination of the resultant TMS ether did not proceed cleanly.
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27
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85033752720
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note
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All new compounds showed satisfactory spectral data.
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