Complexes formed by ZnII, CdII and HgII in the presence of the octadentate ligand 1,4,7,10-tetrakis(pyrazol-1-ylmethyl)-1,4,7,10-tetraazacyclododecane. X-ray structure of the cadmium complex

Polyhedron

Volumn 16, Issue 20, 1997, Pages 3585-3591

  Di Vaira, Massimo ^a   Mani, Fabrizio ^a   Menicatti, Marco ^a   Morassi, Roberto ^a   Stoppioni, Piero ^a  

^a UNIVERSITY OF FLORENCE   (Italy)

Author keywords

Cadmium(II) and mercury(II) complexes; Crystal structure; Functionalized tetraazamacrocycle complexes; Zinc(II)

Indexed keywords

EID: 0011723970     PISSN: 02775387     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0277-5387(97)00117-4     Document Type: Article

References (37)

1. Lindoy, L. F., The Chemistry of Macrocyclic Ligands Complexes, Cambridge University Press, Cambridge, U.K. (1989) ; Parker, D., Pulukkody, K., Norman, T. J., Harrison, A., Royle, L. and Walker, C., J. Chem. Soc., Chem. Commun., 1992, 1441 ; Dhillon, R., Stephens, A. K. W., Whitbread, S. L., Lincoln, S. F. and Wainwright, K. P., J. Chem. Soc., Chem. Commun., 1995, 97.
2. Lindoy, L. F., The Chemistry of Macrocyclic Ligands Complexes, Cambridge University Press, Cambridge, U.K. (1989) ; Parker, D., Pulukkody, K., Norman, T. J., Harrison, A., Royle, L. and Walker, C., J. Chem. Soc., Chem. Commun., 1992, 1441 ; Dhillon, R., Stephens, A. K. W., Whitbread, S. L., Lincoln, S. F. and Wainwright, K. P., J. Chem. Soc., Chem. Commun., 1995, 97.
3. Lindoy, L. F., The Chemistry of Macrocyclic Ligands Complexes, Cambridge University Press, Cambridge, U.K. (1989) ; Parker, D., Pulukkody, K., Norman, T. J., Harrison, A., Royle, L. and Walker, C., J. Chem. Soc., Chem. Commun., 1992, 1441 ; Dhillon, R., Stephens, A. K. W., Whitbread, S. L., Lincoln, S. F. and Wainwright, K. P., J. Chem. Soc., Chem. Commun., 1995, 97.
4. Spirlet, M. R., Rebizant, J., Desreux, J. F. and Loncin, F., Inorg. Chem., 1984, 23, 359; Chang, C. A., Francesconi, L. C., Kumar, K., Malley, M. F., Gougoutas, J. G., Tweedle, M. F., Lee, D. W. and Wilson, J. G., Inorg. Chem., 1993, 32, 3501 ; Parker, D., Pulukkody, K., Smith, F. C., Batsanov, A. and Howard, J. A. K., J. Chem. Soc., Dalton Trans., 1994, 689.
5. Spirlet, M. R., Rebizant, J., Desreux, J. F. and Loncin, F., Inorg. Chem., 1984, 23, 359; Chang, C. A., Francesconi, L. C., Kumar, K., Malley, M. F., Gougoutas, J. G., Tweedle, M. F., Lee, D. W. and Wilson, J. G., Inorg. Chem., 1993, 32, 3501 ; Parker, D., Pulukkody, K., Smith, F. C., Batsanov, A. and Howard, J. A. K., J. Chem. Soc., Dalton Trans., 1994, 689.
6. Spirlet, M. R., Rebizant, J., Desreux, J. F. and Loncin, F., Inorg. Chem., 1984, 23, 359; Chang, C. A., Francesconi, L. C., Kumar, K., Malley, M. F., Gougoutas, J. G., Tweedle, M. F., Lee, D. W. and Wilson, J. G., Inorg. Chem., 1993, 32, 3501 ; Parker, D., Pulukkody, K., Smith, F. C., Batsanov, A. and Howard, J. A. K., J. Chem. Soc., Dalton Trans., 1994, 689.
7. The 'Delfia' system: Soini, E. and Hemmila, I., Clin. Chem., 1979, 25, 353 ; Soini, E., Hemmila, I. and Dahlen, P., Ann. Biol. Clin., 1990, 48, 567; Murru, M., Parker, D., Williams, G. and Beeby, A., J. Chem. Soc., Chem. Commun., 1993, 1116.
8. The 'Delfia' system: Soini, E. and Hemmila, I., Clin. Chem., 1979, 25, 353 ; Soini, E., Hemmila, I. and Dahlen, P., Ann. Biol. Clin., 1990, 48, 567; Murru, M., Parker, D., Williams, G. and Beeby, A., J. Chem. Soc., Chem. Commun., 1993, 1116.
9. The 'Delfia' system: Soini, E. and Hemmila, I., Clin. Chem., 1979, 25, 353 ; Soini, E., Hemmila, I. and Dahlen, P., Ann. Biol. Clin., 1990, 48, 567; Murru, M., Parker, D., Williams, G. and Beeby, A., J. Chem. Soc., Chem. Commun., 1993, 1116.
10. Parker, D. and Jankowski, K. J., Advances in Metals in Medicine (Ed. Abrams, M. J. and Murrer, B. A), Vol. 1, p. 29, Jai Press, New York (1993) ; Parker, D., Chem. Soc. Rev., 1990, 19, 271 ; Broan, C. J., Cox, J. P. L., Craig, A. S., Kataky, R., Parker, D., Harrison, A., Randall, A. M. and Ferguson, G., J. Chem. Soc., Perkin Trans. 2, 1991, 87 ; Parker, D., Pulukkody, K., Smith, F. C., Batsanov, A. and Howard, J. A. K., J. Chem. Soc., Dalton Trans., 1994, 689.
11. Parker, D. and Jankowski, K. J., Advances in Metals in Medicine (Ed. Abrams, M. J. and Murrer, B. A), Vol. 1, p. 29, Jai Press, New York (1993) ; Parker, D., Chem. Soc. Rev., 1990, 19, 271 ; Broan, C. J., Cox, J. P. L., Craig, A. S., Kataky, R., Parker, D., Harrison, A., Randall, A. M. and Ferguson, G., J. Chem. Soc., Perkin Trans. 2, 1991, 87 ; Parker, D., Pulukkody, K., Smith, F. C., Batsanov, A. and Howard, J. A. K., J. Chem. Soc., Dalton Trans., 1994, 689.
12. Parker, D. and Jankowski, K. J., Advances in Metals in Medicine (Ed. Abrams, M. J. and Murrer, B. A), Vol. 1, p. 29, Jai Press, New York (1993) ; Parker, D., Chem. Soc. Rev., 1990, 19, 271 ; Broan, C. J., Cox, J. P. L., Craig, A. S., Kataky, R., Parker, D., Harrison, A., Randall, A. M. and Ferguson, G., J. Chem. Soc., Perkin Trans. 2, 1991, 87 ; Parker, D., Pulukkody, K., Smith, F. C., Batsanov, A. and Howard, J. A. K., J. Chem. Soc., Dalton Trans., 1994, 689.
13. Parker, D. and Jankowski, K. J., Advances in Metals in Medicine (Ed. Abrams, M. J. and Murrer, B. A), Vol. 1, p. 29, Jai Press, New York (1993) ; Parker, D., Chem. Soc. Rev., 1990, 19, 271 ; Broan, C. J., Cox, J. P. L., Craig, A. S., Kataky, R., Parker, D., Harrison, A., Randall, A. M. and Ferguson, G., J. Chem. Soc., Perkin Trans. 2, 1991, 87 ; Parker, D., Pulukkody, K., Smith, F. C., Batsanov, A. and Howard, J. A. K., J. Chem. Soc., Dalton Trans., 1994, 689.
14. Dubost, J. P., Leger, M., Langlois, M. H., Meyer, D. and Schaefer, M. C., C.R. Acad. Sci., Paris Ser. 2, 1991, 312, 349; Norman, T. J., Parker, D., Royle, L., Harrison, A., Antoniw, P. and King, D. J., J. Chem. Soc., Chem. Commun., 1995, 1877.
15. Dubost, J. P., Leger, M., Langlois, M. H., Meyer, D. and Schaefer, M. C., C.R. Acad. Sci., Paris Ser. 2, 1991, 312, 349; Norman, T. J., Parker, D., Royle, L., Harrison, A., Antoniw, P. and King, D. J., J. Chem. Soc., Chem. Commun., 1995, 1877.
16. Carlton, L., Hancock, R. D., Maumela, H. and Wainwright, K. P., J. Chem. Soc., Dalton Trans., 1994, 1007.
17. Buoen, S., Dale, J., Groth, P. and Krane, J., J. Chem. Soc., Chem. Commun., 1982, 1172; Turonek, M. L., Clarke, P., Laurence, G. S., Lincoln, S. F., Pittet, P.-A., Politis, S. and Wainwright, K. P., Inorg. Chem., 1993, 32, 2195; Stephens, A. K. W. and Lincoln, S. F., J. Chem. Soc., Dalton Trans., 1993, 2123.
18. Buoen, S., Dale, J., Groth, P. and Krane, J., J. Chem. Soc., Chem. Commun., 1982, 1172; Turonek, M. L., Clarke, P., Laurence, G. S., Lincoln, S. F., Pittet, P.-A., Politis, S. and Wainwright, K. P., Inorg. Chem., 1993, 32, 2195; Stephens, A. K. W. and Lincoln, S. F., J. Chem. Soc., Dalton Trans., 1993, 2123.
19. Buoen, S., Dale, J., Groth, P. and Krane, J., J. Chem. Soc., Chem. Commun., 1982, 1172; Turonek, M. L., Clarke, P., Laurence, G. S., Lincoln, S. F., Pittet, P.-A., Politis, S. and Wainwright, K. P., Inorg. Chem., 1993, 32, 2195; Stephens, A. K. W. and Lincoln, S. F., J. Chem. Soc., Dalton Trans., 1993, 2123.
20. (a) Aime, S., Botta, M. and Ermondi, G., Inorg. Chem., 1992, 31, 4291;
21. (b) Aime, S., Barge, A., Botta, M., Fasano, M., Ayala, J. D. and Bombieri, G., Inorg. Chim. Acta, 1996, 246, 423 ;
22. (c) Stephens, A. K. W., Dhillon, R., Lincoln, S. F. and Wainwright, K. P., Inorg. Chim. Acta, 1995, 236, 185;
23. (d) Dhillon, R., Stephens, A. K. W., Whitbread, S. L., Lincoln, S. F. and Wainwright, K. P., J. Chem. Soc., Chem. Commun., 1995, 97;
24. (e) Carlton, L., Hancock, R. D., Maumela, H. and Wainwright, K. P., J. Chem. Soc., Chem. Commun., 1994, 1007;
25. (f) Clarke, P., Hounslow, A. M., Keough, R. A., Lincoln, S. F. and Wainwright, K. P., Inorg. Chem., 1990, 29, 1793;
26. (g) Parker, D. and Williams, J. A. G., J. Chem. Soc., Dalton Trans., 1996, 3613.
27. Di Vaira, M., Mani, F., Nardi, N., Stoppioni, P. and Vacca, A., J. Chem. Soc., Dalton Trans., 1996, 2679.
28. De Martino Norante, G., Di Vaira, M., Mani, F., Mazzi, S. and Stoppioni, P., Inorg. Chem., 1990, 29, 2822.
29. (a) De Martino Norante, G., Di Vaira, M., Mani, F., Mazzi, S. and Stoppioni, P., J. Chem. Soc., Chem. Commun., 1990, 438;
30. (b) Cosimelli, B., Di Vaira, M., Mani, F. and Stoppioni, P., J. Chem. Soc., Dalton Trans., 1991, 331.
31. Di Vaira, M., Mani, F. and Stoppioni, P., J. Chem. Soc., Dalton Trans., 1992, 1127.
32. Sheldrick, G. M., SHELX 76, Program for Crystal Structure Determination, University of Cambridge, 1976.
33. Walker, N. and Stuart, D., Acta Cryst., Sect. A, 1983, 39, 158.
34. International Tables for X-Ray Crystallography, p. 99. vol. 4, Kynoch Press, Birmingham, U.K. (1974).
35. Ref. 15, p. 149.
36. Shannon, R. D. and Prewitt, C. T., Acta Cryst., Sect. B., 1969, 25, 925.
37. Maumela, H., Hancock, R. D., Carlton, L., Reibenspies, J. H. and Wainwright, K. P., J. Am. Chem. Soc., 1995, 117, 6698.