Generation of ethyl metathiophosphate by thermal fragmentation of O-ethyl N-substituted phosphoramidothioates

Journal of Organic Chemistry

Volumn 61, Issue 12, 1996, Pages 3944-3950

  Quin, Louis D ^a   Hermann, Petr ^a,c   Jankowski, Stefan ^b  

^a UNIVERSITY OF MASSACHUSETTS   (United States)

^b LODZ UNIVERSITY OF TECHNOLOGY   (Poland)

^c CHARLES UNIVERSITY   (Czech Republic)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0010948018     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo952270j     Document Type: Article

References (22)

1. Quin, L. D.; Jankowski, S. J. Org. Chem. 1994, 59, 4402.
2. Jankowski, S.; Quin, L. D.; Paneth, P.; O'Leary, M. H. J. Am. Chem. Soc. 1994, 116, 11675.
3. This aspect of metaphosphate chemistry has recently been reviewed, see: Quin, L. D. Coord. Chem. Rev. 1994, 137, 525.
4. Quin, L. D.; Sadanani, N. D.; Wu, X.-P. J. Am. Chem. Soc. 1989, 111, 6852.
5. Quin, L. D.; Wu, X.-P.; Sadanani, N. D.; Lukes, I.; Ionkin, A. S.; Day, R. O. J. Org. Chem. 1994, 59, 120.
6. Bodalski, R.; Jankowski, S.; Glówka, M. L.; Filipiak, T.; Quin, L. D. J. Org. Chem. 1994, 59, 5173.
7. Freeman, S.; Harger, J. P. J. Chem. Soc., Perkin Trans 2 1988, 81.
8. Piotto, M. E.; Granger, J. N.; Cho, Y.; Farschtschi, N.; Gorenstein, D. G. Tetrahedron 1991, 47, 2449.
9. Tebby, J. C. Handbook of Phosphorus-31 Nuclear Magnetic Resonance Data; CRC Press: Boca Raton, FL, 1991; pp 257-259.
10. Mastryukova, T. A. Phosphorus, Sulfur Silicon Relat. Elem. 1976, 1, 211.
11. Mahmood, T.; Shreeve, J. M. Inorg. Chem. 1986, 25, 3830.
12. Chasar, D. W.; Fackler, J. F., Jr.; Komoroski, R. A.; Kroenke, W. J.; Mazany, A. M. J. Am. Chem. Soc. 1986, 108, 5956.
13. Jankowski, S.; Chen, S.; Quin, L. D. Unpublished results.
14. Jankowski, S.; Paneth, P.; O'Leary, M. H.; Quin, L. D. Unpublished results.
15. Quin, L. D. In Phosphorus-31 NMR Spectral Properties in Compound Characterization and Structural Analysis; Quin, L. D., Verkade, J. G., Eds.; VCH Publishers: New York, 1994; Chapter 32.
16. Quin, L. D.; Wu, X.-P.; Quin, G. S.; Jankowski, S. Phosphorus, Sulfur Silicon Relat. Elem. 1993, 76, 91.
17. Lukes, I.; Borbaruah, M.; Quin, L. D. J. Am. Chem. Soc. 1994, 116, 1737.
18. Quin, L. D.; Hermann, P. Unpublished results.
19. Fletcher, J. H.; Hamilton, J. C.; Hechenbleikner, I.; Hoegberg, E.; Serti, B. J.; Cassaday, J. T. J. Am. Chem. Soc. 1948, 70, 3943.
20. Michalski, J.; Reimschüssel, W.; Kaminski, R. Russ. Chem. Rev. 1978, 47, 814.
21. Instruments and general techniques are described in refs 1 and 22.
22. Jankowski, S.; Quin, L. D. J. Am. Chem. Soc. 1991, 113, 7011.