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Volumn 16, Issue 20, 1997, Pages 4299-4313

Osmium alkyl and silyl derivatives with cyclopentadienyl(phosphine) and pentamethylcyclopentadienyl(phosphine) ligand sets

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EID: 0010927888     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om9704197     Document Type: Article
Times cited : (44)

References (112)
  • 1
    • 0003067989 scopus 로고
    • Patai, S., Rappoport, Z., Eds.; Wiley: New York, Chapters 9, 10
    • For reviews of metal-silicon compounds, see: (a) Tilley, T. D. In The Silicon-Heteroatom Bond; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1991; Chapters 9, 10, pp 245, 309. (b) Tilley, T. D. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1989; Chapter 24, p 1415. (c) Mackay, K. M.; Nicholson, B. K. In Comprehensive Organometallic Chemistry; Wilkinson, G. , Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: Oxford, 1982; Vol. 6, p 1043. (d) Aylett, B. J. Adv. Inorg. Chem. Radiochem. 1982, 25, 1. (e) Pannell, K. H.; Sharma, H. K. Chem. Rev. 1995, 95, 1351. (f) Schubert, U. Angew. Chem., Int. Ed. Engl. 1994, 33, 419.
    • (1991) The Silicon-Heteroatom Bond , pp. 245
    • Tilley, T.D.1
  • 2
    • 0001418043 scopus 로고
    • Patai, S., Rappoport, Z., Eds.; Wiley: New York, Chapter 24
    • For reviews of metal-silicon compounds, see: (a) Tilley, T. D. In The Silicon-Heteroatom Bond; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1991; Chapters 9, 10, pp 245, 309. (b) Tilley, T. D. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1989; Chapter 24, p 1415. (c) Mackay, K. M.; Nicholson, B. K. In Comprehensive Organometallic Chemistry; Wilkinson, G. , Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: Oxford, 1982; Vol. 6, p 1043. (d) Aylett, B. J. Adv. Inorg. Chem. Radiochem. 1982, 25, 1. (e) Pannell, K. H.; Sharma, H. K. Chem. Rev. 1995, 95, 1351. (f) Schubert, U. Angew. Chem., Int. Ed. Engl. 1994, 33, 419.
    • (1989) The Chemistry of Organic Silicon Compounds , pp. 1415
    • Tilley, T.D.1
  • 3
    • 84942776708 scopus 로고
    • Wilkinson, G. , Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: Oxford
    • For reviews of metal-silicon compounds, see: (a) Tilley, T. D. In The Silicon-Heteroatom Bond; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1991; Chapters 9, 10, pp 245, 309. (b) Tilley, T. D. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1989; Chapter 24, p 1415. (c) Mackay, K. M.; Nicholson, B. K. In Comprehensive Organometallic Chemistry; Wilkinson, G. , Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: Oxford, 1982; Vol. 6, p 1043. (d) Aylett, B. J. Adv. Inorg. Chem. Radiochem. 1982, 25, 1. (e) Pannell, K. H.; Sharma, H. K. Chem. Rev. 1995, 95, 1351. (f) Schubert, U. Angew. Chem., Int. Ed. Engl. 1994, 33, 419.
    • (1982) Comprehensive Organometallic Chemistry , vol.6 , pp. 1043
    • Mackay, K.M.1    Nicholson, B.K.2
  • 4
    • 4243193337 scopus 로고
    • For reviews of metal-silicon compounds, see: (a) Tilley, T. D. In The Silicon-Heteroatom Bond; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1991; Chapters 9, 10, pp 245, 309. (b) Tilley, T. D. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1989; Chapter 24, p 1415. (c) Mackay, K. M.; Nicholson, B. K. In Comprehensive Organometallic Chemistry; Wilkinson, G. , Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: Oxford, 1982; Vol. 6, p 1043. (d) Aylett, B. J. Adv. Inorg. Chem. Radiochem. 1982, 25, 1. (e) Pannell, K. H.; Sharma, H. K. Chem. Rev. 1995, 95, 1351. (f) Schubert, U. Angew. Chem., Int. Ed. Engl. 1994, 33, 419.
    • (1982) Adv. Inorg. Chem. Radiochem. , vol.25 , pp. 1
    • Aylett, B.J.1
  • 5
    • 0000835395 scopus 로고
    • For reviews of metal-silicon compounds, see: (a) Tilley, T. D. In The Silicon-Heteroatom Bond; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1991; Chapters 9, 10, pp 245, 309. (b) Tilley, T. D. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1989; Chapter 24, p 1415. (c) Mackay, K. M.; Nicholson, B. K. In Comprehensive Organometallic Chemistry; Wilkinson, G. , Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: Oxford, 1982; Vol. 6, p 1043. (d) Aylett, B. J. Adv. Inorg. Chem. Radiochem. 1982, 25, 1. (e) Pannell, K. H.; Sharma, H. K. Chem. Rev. 1995, 95, 1351. (f) Schubert, U. Angew. Chem., Int. Ed. Engl. 1994, 33, 419.
    • (1995) Chem. Rev. , vol.95 , pp. 1351
    • Pannell, K.H.1    Sharma, H.K.2
  • 6
    • 33748214668 scopus 로고
    • For reviews of metal-silicon compounds, see: (a) Tilley, T. D. In The Silicon-Heteroatom Bond; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1991; Chapters 9, 10, pp 245, 309. (b) Tilley, T. D. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1989; Chapter 24, p 1415. (c) Mackay, K. M.; Nicholson, B. K. In Comprehensive Organometallic Chemistry; Wilkinson, G. , Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: Oxford, 1982; Vol. 6, p 1043. (d) Aylett, B. J. Adv. Inorg. Chem. Radiochem. 1982, 25, 1. (e) Pannell, K. H.; Sharma, H. K. Chem. Rev. 1995, 95, 1351. (f) Schubert, U. Angew. Chem., Int. Ed. Engl. 1994, 33, 419.
    • (1994) Angew. Chem., Int. Ed. Engl. , vol.33 , pp. 419
    • Schubert, U.1
  • 7
    • 0000829913 scopus 로고
    • Patai, S., Rappoport, Z., Eds.; Wiley: New York, Chapter 25
    • For a review of hydrosilation, see: Ojima, I. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; Wiley: New York, 1989; Chapter 25, p 1479.
    • (1989) The Chemistry of Organic Silicon Compounds , pp. 1479
    • Ojima, I.1
  • 9
    • 85033189960 scopus 로고
    • Zeldin, M., Wynne, K. J., Allcock, H. R., Eds.; ACS Symposium Series 360; American Chemical Society: Washington, DC, Chapter 7
    • (b) Harrod, J. F. In Inorganic and Organometallic Polymers; Zeldin, M., Wynne, K. J., Allcock, H. R., Eds.; ACS Symposium Series 360; American Chemical Society: Washington, DC, 1988; Chapter 7.
    • (1988) Inorganic and Organometallic Polymers
    • Harrod, J.F.1
  • 12
    • 0000806201 scopus 로고
    • Larson, G., Ed.; JAI Press, Inc.: Greenwich, CT
    • (e) Corey, J. In Advances in Silicon Chemistry; Larson, G., Ed.; JAI Press, Inc.: Greenwich, CT, 1991; Vol. 1, p 327.
    • (1991) Advances in Silicon Chemistry , vol.1 , pp. 327
    • Corey, J.1
  • 55
    • 0004099399 scopus 로고
    • Plenum Press: New York
    • (a) Multinuclear NMR; Mason, J., Ed.; Plenum Press: New York, 1987.
    • (1987) Multinuclear NMR
    • Mason, J.1
  • 56
  • 62
    • 3743078763 scopus 로고
    • Wilkinson, G., Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: London, Chapter 39
    • For reviews on orthometalation, see: (a) Hartley, F. R. In Comprehensive Organometallic Chemistry; Wilkinson, G., Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: London, 1982; Vol. 6, Chapter 39, p 592. (b) Ryabov, A. D. Chem. Rev. 1990, 90, 403.
    • (1982) Comprehensive Organometallic Chemistry , vol.6 , pp. 592
    • Hartley, F.R.1
  • 63
    • 0042728760 scopus 로고
    • For reviews on orthometalation, see: (a) Hartley, F. R. In Comprehensive Organometallic Chemistry; Wilkinson, G., Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: London, 1982; Vol. 6, Chapter 39, p 592. (b) Ryabov, A. D. Chem. Rev. 1990, 90, 403.
    • (1990) Chem. Rev. , vol.90 , pp. 403
    • Ryabov, A.D.1
  • 70
    • 85033171951 scopus 로고
    • Ph.D. Thesis, University of California, San Diego, CA
    • Grumbine, S. K. Ph.D. Thesis, University of California, San Diego, CA, 1993.
    • (1993)
    • Grumbine, S.K.1
  • 71
    • 0001043284 scopus 로고    scopus 로고
    • Isomers D and E can be interconverted by two cycles of a combined Berry-turnstile mechanism, see: Smith, J. M.; Coville, N. J. Organometallics 1996, 15, 3388.
    • (1996) Organometallics , vol.15 , pp. 3388
    • Smith, J.M.1    Coville, N.J.2
  • 72
    • 85033181481 scopus 로고    scopus 로고
    • note
    • A search of the Cambridge Structural Database revealed a mean Os-Si single bond length of 2.40(2) Å.
  • 88
    • 85033172541 scopus 로고    scopus 로고
    • note
    • 2OTf (ref 6c).
  • 112
    • 85033176256 scopus 로고    scopus 로고
    • note
    • The reaction will not work with complete exclusion of water, and a much longer reaction time is required (with lower yield of product) when less than 25 mL of water is added to the reaction mixture.


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