Fast Synthesis of Aryl Triflates with Controlled Microwave Heating

Organic Letters

Volumn 4, Issue 7, 2002, Pages 1231-1233

  Bengtson, Anna ^a   Hallberg, Anders ^a   Larhed, Mats ^a  

^a UPPSALA UNIVERSITY   (Sweden)

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ARTICLE;

EID: 0009860642     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol025701a     Document Type: Article

References (12)

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3. (c) Lew, A.; Krutzik, P. O.; Hart, M. E.; Chamberlin, A. R. J. Comb. Chem. 2002, 4, 95-105.
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8. (b) Wentworth, A. D.; Wentworth, P., Jr.; Mansoor, U. F.; Janda, K. D. Org. Lett. 2000, 2, 477-480.
9. Subramanian, L. R.; Hanack, M.; Chang, L. W. K.; Imhoff, M. A.; Schleyer, P. v. R.; Effenberger, F.; Kurtz, W.; Stang, P. J.; Dueber, T. E. J. Org. Chem. 1976, 41, 4099-4103.
10. 3 (6.0 mmol, 830 mg), and 3.0 mL of THF were mixed in a septum-capped tube. The reaction mixture was heated to 120°C for 6 min in a SmithSynthesizer.
11. Barlos, K.; Chatzi, O.; Gatos, D.; Stavropoulos, G. Int. J. Peptide Protein Res. 1991, 37, 513-520.
12. Tan δ = 0.047 at room temperature; Gabriel, C.; Gabriel, S.; Grant, E. H.; Halstead, B. S. J.; Mingos, D. M. P. Chem. Soc. Rev. 1998, 27, 213-224.