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Volumn 2, Issue 9, 2000, Pages 1319-1322

Asymmetric desymmetrization of 2,2′,6,6′-tetrahydroxybiphenyl through annulation with enantiomerically pure bis(mesylate)

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EID: 0008757162     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol0057840     Document Type: Article
Times cited : (34)

References (41)
  • 1
    • 0002350886 scopus 로고
    • For review on the nonenzymatic method, see: (a) Ward, R. S. Chem. Soc. Rev. 1990. 19, 1.
    • (1990) Chem. Soc. Rev. , vol.19 , pp. 1
    • Ward, R.S.1
  • 2
    • 0006198233 scopus 로고
    • Helmchen, G., Hoffmann, R. W., Mulzer, J., Schumann, E., Eds.; Georg Thieme Verlag: Stuttgart
    • (b) Gais, H.-J. Methods of Organic Chemistry (Houben-Weyl); Helmchen, G., Hoffmann, R. W., Mulzer, J., Schumann, E., Eds.; Georg Thieme Verlag: Stuttgart, 1995; Vol. E21a, p 589.
    • (1995) Methods of Organic Chemistry (Houben-Weyl) , vol.E21A , pp. 589
    • Gais, H.-J.1
  • 3
    • 85037512423 scopus 로고
    • For recent reports
    • (c) Harada, T.; Oku, A. Synlett 1994, 95. For recent reports, see:
    • (1994) Synlett , pp. 95
    • Harada, T.1    Oku, A.2
  • 4
    • 0033214275 scopus 로고    scopus 로고
    • and references therein. For enzymatic methods
    • (d) Harada, T.; Nakamura, T.; Kinugasa, M.; Oku, A. J. Org. Chem. 1999, 64, 7594 and references therein. For enzymatic methods, see:
    • (1999) J. Org. Chem. , vol.64 , pp. 7594
    • Harada, T.1    Nakamura, T.2    Kinugasa, M.3    Oku, A.4
  • 13
    • 0000332467 scopus 로고
    • Helmchen, G., Hoffmann, R. W., Mulzer, J., Schumann, E., Eds.; Georg Thieme Verlag: Stuttgart
    • (b) Review: Bringmann, G.; Walter, R.; Weirich, R. Methods of Organic Chemistry (Houben-Weyl); Helmchen, G., Hoffmann, R. W., Mulzer, J., Schumann, E., Eds.; Georg Thieme Verlag: Stuttgart, 1995; Vol. E21a, p 567.
    • (1995) Methods of Organic Chemistry (Houben-Weyl) , vol.E21A , pp. 567
    • Bringmann, G.1    Walter, R.2    Weirich, R.3
  • 31
    • 85037515619 scopus 로고    scopus 로고
    • note
    • The symbol "a" indicates the axial chirality. Thus, "aS.R" shows that the compound has aS-axial chirality and an R-stereogenic center.
  • 34
    • 85037514750 scopus 로고    scopus 로고
    • note
    • 4: C, 69.76; H, 5.46. Found: C, 69.57; H, 5.52.
  • 35
    • 85037513146 scopus 로고    scopus 로고
    • note
    • The ee value was established by HPLC analyses using a Chiracel AD column with 90:10:0.09 hexane:2-propanol:acetic acid as a mobile phase at a flow rate of 1 mL/min.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.