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5244310514
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note
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Data for 3 were collected on a Rigaku AFC5R rotating anode diffractometer. The TEXSAN suite of programs were used for data collection and data processing, Molecular Structure Corp.: Woodlands, TX. Data for 6 were collected on a Siemens SMART IK CCD diffractometer. The SMART v4.05 and SAINT v4.05 programs were used for data collection and data processing, Siemens Analytical X-ray Instruments, Inc.: Madison, WI. SADABS was used for the application of a semiempirical absorption correction, G. M. Sheldrick, University of Goettingen, Germany. Data for 12 were collected on a Siemens P4 diffractometer. The XSCANS suite of programs were used for data collection and data processing, Siemens Analytical X-ray Instruments, Inc.: Madison, WI.
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5244336432
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note
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SHEXLXTL v5.03 was used for the structure solution and generation of figures and tables, Siemens Analytical X-ray Instruments, Inc.: Madison, WI. Neutral-atom scattering factors were used as stored in SHELXTL v5.03.
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45
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5244224172
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note
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(3T) SQUEEZE is a routine implemented in PLATON-92, which allows solvent contributions to be eliminated from the reflection data. A. L. Spek, University of Utrecht, Utrecht, The Netherlands.
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Molecular Simulations Inc.: San Diego, April
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