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Volumn 29, Issue 26, 1988, Pages 3235-3238

Phosphinites from cinchona alkaloids; catalytic application in hydrosilylation reaction

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0008444820 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/0040-4039(88)85130-X Document Type: Article

Times cited : (25)

References (25)

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- Morrison¹

3
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- VCH Publishers, New-York
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- Nogradi¹

4
- 0003905731
- J.D Morrison, Academic Press, Inc, New-York
- (1985) Asymmetric Synthesis , vol.5
- Kagan¹

6
- 85050272509
- E.L Eliel, S.H Wilem, N.L Allinger, J. Wiley
- (1986) Topics in Stereochemistry , vol.16 , pp. 87
- Wynberg¹

7
- 0001559784
- (1984) Organometallics , vol.3 , pp. 1354
- Brunner¹ Becker² Riepl³

8
- 84918430800
- Int. Ed. Engl.
- (1983) Angew. Chem. , vol.22 , pp. 33
- Brunner¹ Riepl² Weitzer³

9
- 84981969955
- Asymmetric Hydrosilylation of Acetophenone with Rhodium-Complexes of Optically Active Schiff Bases
- Int. Ed. Engl.
- (1982) Angewandte Chemie International Edition in English , vol.5 , pp. 377
- Brunner¹ Riepl²

10
- 84981925727
- Asymmetrische Hydrosilylierung von Acetophenon mit Rhodium-Komplexen optisch aktiver Schiff-Basen
- (1982) Angewandte Chemie International Edition in English , pp. 769
- Brunner¹ Riepl²

11
- 0001048411
- J.D Morrison, Academic Press, Inc, New-York
- (1985) Asymmetric Synthesis , vol.5 , pp. 104
- Ojima¹ Hirai²

12
- 85026814650
- E.L Eliel, S.H Wilem, N.L Allinger, J. Wiley
- (1984) Topics in Stereochemistry , vol.15 , pp. 43
- Corriu¹ Guerin² Moreau³

13
- 0001226611
- Asymmetric hydrosiliylation of ketones, catalyzed by rhodium complexes containing chiral chelate ligands. Crystal and molecular structure of (bicyclo[2.2.1]hepta-2,5-diene)[(S)-N,N-dimethyl-1-[o-(diphenylarsino)phenyl]ethylamine]rhodium(I) perchlorate
- (1982) Inorganic Chemistry , vol.21 , pp. 185
- Payne¹ Stephan²

14
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- (1981) J. Mol. Catal. , vol.12 , pp. 37
- Johnson¹ Klein² Thomen³

15
- 0001227225
- (1974) Tetrahedron Lett. , vol.49 , pp. 4405
- Hayashi¹ Yamamoto² Kumada³

16
- 0346588298
- (1986) Tetrahedron lett. , vol.27 , pp. 345
- Karim¹ Mortreux² Petit³

17
- 84918456057
- Phosphinite synthesis: To a well-stirred solution of the alkaloid (6.38 g, 0.02 mol) in dry degassed tetrahydrofuran (50 ml) under nitrogen, was introduced butyllithium (13.3 ml of 1.5 M solution in hexane, 0.02 mol), followed by the slow introduction of chlorodiphenylphosphine (4.41 g, 0.02 ml; freshly distilled and stored under nitrogen). After 15 min stirring at room temperature, the solvents were evaporated and the crude product was obtained quantitatively (with one equivalent of lithium chloride) as a white or yellow powder.

18
- 0002167071
- Optically active phosphines : New synthetic approach
- 31P = 29 ; 34 ; −22 and −156 ppm.
- (1979) Tetrahedron Letters , vol.12 , pp. 1069
- Chodkiewicz¹ Jore² Wodzki³

19
- 84918456056
- Phosphinite ligands free of lithium salts were obtained by flash chromatography under nitrogen atmosphere, on a silicagel column, eluant dry and degassed ethyl acetate.

20
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- F Wilkinson, G.A Stone, E.W Abel
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- Kagan¹

22
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- Gas chromatographic enantiomer separation of chiral alcohols
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- König¹ Franke² Beneke³

23
- 33845280103
- See, on Asymmetric Dihydroxylation via Ligand-Accelerated Catalysis.
- (1988) J. Am. Chem. Soc. , vol.110 , pp. 1968
- Jacobsen¹ Markò² Mungall³ Schröder⁴ Sharpless⁵

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