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Tetrahedron Letters

Volumn 28, Issue 13, 1987, Pages 1443-1446

Stereoselective synthesis of (E)-alkenylsilanes from aldehydes with a reagent prepared by chromium(II) reduction of Me3SiCHBr2

(4) Takai, Kazuhiko a Kataoka, Yasutaka a Okazoe, Takashi a Utimoto, Kiitiro a

a KYOTO UNIVERSITY (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0007850846 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)95949-5 Document Type: Article

Times cited : (77)

References (28)

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27
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- 2 (0.98 g, 8.0 mmol) in THF (20 mL). In the case of nonanal, a THF solution of LiI (1.0 M, 4.0 mmol) is added to the mixture successively (ref. 13). After stirring at 25°C for the number of hours shown in scheme 3, the mixture is subjected to an aqueousworkup. Purification of the crude product by preparative TLC onsilica gel affords the desired vinyl sulfide.

28
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- 30OSi: C, 70.79; H, 11.88%.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.