Convenient route to niobium in lower oxidation states: Synthesis and crystal structure of K4[Nb(C2O4)4]·4H 2O·1/2H2C2O4

Inorganica Chimica Acta

Volumn 266, Issue 1, 1997, Pages 103-107

  Ooi, Bee Lean ^a   Shihabara, Takashi ^b   Sakane, Genta ^b   Mok, Kum Fun ^a  

^a NATIONAL UNIVERSITY OF SINGAPORE   (Singapore)

^b OKAYAMA UNIVERSITY OF SCIENCE   (Japan)

Author keywords

Crystal structures; Niobium complexes; Octa coordinate complexes; Oxalate complexes

Indexed keywords

COMPLEXATION; COORDINATION REACTIONS; CRYSTAL STRUCTURE; OXALIC ACID; X RAY CRYSTALLOGRAPHY;

AQUEOUS SOLUTION CHEMISTRY; COORDINATE COMPLEXES; ETHANOL SOLUTIONS; NIOBIUM COMPLEXES; NIOBIUM PENTACHLORIDE; OXALATE COMPLEXES; OXIDATION STATE; SYNTHESIS AND CRYSTAL STRUCTURE;

NIOBIUM COMPOUNDS;

EID: 0007761534     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/s0020-1693(97)05526-6     Document Type: Article

References (30)

1. L.G. Hubert-Pfalzraf, M. Postel and J.G. Riess, Niobium and tantalum, in G. Wilkinson, R.D. Gillard and J.A. McCleverty (eds.), Comprehensive Coordination Chemistry, Vol. 3, Pergamon, 1985, Ch. 34.
2. F. Ott, Elektrochem. Z., 18 (1912) 349.
3. S.J. Kiehl and H.B. Hardt, J. Am. Chem. Soc., 50 (1928) 1608 and 2337.
4. S.J. Kiehl, R.L. Fox and H.B. Hardt, J. Am. Chem. Soc., 4 (1937) 1138.
5. E.W. Golibersuch and R.C. Young, J. Am. Chem. Soc., 71 (1949) 2402.
6. E.I. Krylov, N.N. Kalugina and J. Russ., Inorg. Chem., 4 (1959) 1138.
7. Y.G. Goroshchenko, M.I. Andreeva and J. Russ, Inorg. Chem., 11 (1966) 1197.
8. A. Bino, J. Am. Chem. Soc., 102 (1980) 7991; Inorg. Chem., 21 (1982) 1917.
9. A. Bino, J. Am. Chem. Soc., 102 (1980) 7991; Inorg. Chem., 21 (1982) 1917.
10. D. Cozzi and S. Vivarelli, Z. Anorg. Allg. Chem., 279 (1955) 165.
11. V.N. Fedotov, N.S. Garif'yanov and B.M. Kozyrev, Dokl. Akad. Nauk. SSSR, 145 (1962) 1318.
12. M. Lardon and H.H. Gunthard, J. Chem. Phys., 44 (1966) 2010.
13. I.F. Gainullin, N.S. Garif'yanov and B.M. Kozyrev, Dokl. Akad. Nauk. SSSR, 180 (1968) 858.
14. R.A.D. Wentworth and C.H. Brubaker, Jr., Inorg. Chem., 1 (1962) 971; 2 (1963) 551.
15. R.A.D. Wentworth and C.H. Brubaker, Jr., Inorg. Chem., 1 (1962) 971; 2 (1963) 551.
16. F.A. Cotton, S.A. Duraj and W.J. Roth, J. Am. Chem. Soc., 106 (1984) 3527.
17. F.A. Cotton, M.P. Diebold, M. Matusz and W.J. Roth, Inorg. Chim. Acta, 112 (1986) 147.
18. F.A. Cotton, M.P. Diebold, R. Llusar and W.J. Roth, J. Chem. Soc., Chem. Commun., (1986) 1276.
19. F.A. Cotton, M.P. Diebold and W.J. Roth, Inorg. Chem., 26 (1987) 3323.
20. F.A. Cotton, M.P. Diebold and W.J. Roth, Inorg. Chem., 27 (1988) 2347.
21. E. Babaian-Kibala, F.A. Cotton and M. Shang, Inorg. Chem., 29 (1990) 5148.
22. F.A. Cotton, M.P. Diebold and W.J. Roth, Inorg. Chem., 24 (1985) 3509.
23. S.H. Chan and B.L. Ooi, Transition Met. Chem., 18 (1993) 473.
24. G. Mathern, R. Weiss and R.J. Rohmer, J. Chem. Soc., Chem. Commun., (1969) 70.
25. N. GaLesic, B. Matkovic and M. Herceg, J. Less-Common Met., 25 (1971) 234.
26. F.A. Cotton, M.P. Diebold and W.J. Roth, Inorg. Chem., 26 (1987) 2889.
27. S. Minhas and D.T. Richens, J. Chem. Soc., Dalton Trans., (1996) 703.
28. S.J. Lippard, Prog. Inorg. Chem., 8 (1967) 109.
29. T.J. Pinnavaia, B.L. Barnett, G. Podolsky and A. Tulinsky, J. Am. Chem. Soc., 97 (1975) 2712.
30. E.L. Muetterties and L.J. Guggenberger, J. Am. Chem. Soc., 96 (1974) 1748.