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For a recent review, see C. M. Paleos and D. Tsiourvas, Angew. Chem., Int. Ed. Engl., 1995, 34, 1696.
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3
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(a) D. W. Bruce, D. A. Dunmur, E. Lalinde, P. M. Maitlis and P. Styring, Liq. Cryst., 1988, 3, 385.
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Bruce, D.W.1
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4
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2542603753
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in the press
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(b) H. C. Lin, L. L. Lai, Y. S. Lin, C. Tsai and R. C. Chen, Mol. Cryst. Liq. Cryst., 1998, in the press.
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5
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27844454039
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note
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6 suffered the limitations of low overall yield and/or delicate synthetic operations.
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7
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0002508797
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Chemistry of Thienothiophenes
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eds. A. R. Katritzky and A. J. Boulton, Academic Press, New York
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V. P. Litvinov and Y. A. L. Gol'dfarb, Chemistry of Thienothiophenes, in Advanced Heterocyclic Chemistry, eds. A. R. Katritzky and A. J. Boulton, Academic Press, New York, 1976, 19, 123.
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Litvinov, V.P.1
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J. D. Prugh, G. D. Hartman, P. J. Mallorga, B. M. McKeever, S. R. Michelson, M. A. Murcko, H. Schwam, R. L. Smith, J. M. Sondey, J. P. Springer and M. F. Sugrue, J. Med. Chem., 1991, 34, 1805.
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Prugh, J.D.1
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10
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0001688531
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Y. Fujimoto and T. Tatsuno, Tetrahedron Lett., 1976, 3325. The use of Zn-Ag instead of the zinc powder in our system greatly improved the yield of 5 (from 55% to 80%).
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Fujimoto, Y.1
Tatsuno, T.2
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11
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27844594551
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note
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Ketals 7 and 8 are stable enough on silica gel and can be isolated by flash chromatography (silica gel, EtOAc-hexane, 1 : 25 for 7, 1 : 35 for 8).
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13
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27844584461
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note
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For several carboxylic acids with mesogenic properties due to the dimeric acid association through hydrogen bonding, see ref. 1.
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15
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0000653651
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D. J. Price, K. Willis, T. Richardson, G. Ungar and D. W. Bruce, J. Mater. Chem., 1997, 7, 883;
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T. Kato, H. Adachi, A. Fujishima and J. M. J. Frechet, Chem. Lett., 1992, 265;
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0002909019
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K. Willis, J. E. Luckhurst, D. J. Price, J. M. J. Frechet, J. Kihara, T. Kato, G. Ungar and D. W. Bruce, Liq. Cryst., 1996, 21, 585.
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