Synthesis of [Cu2(Me2[9]aneN2S)2(OH)2] (PF6)2, a hydroxo-bridged copper(II) complex of N,N′- dimethyl-1-thia-4,7-diazacyclononane (Me2[9]aneN2S). X-ray structural analysis. Magnetic susceptibility, E.P.R. and visible spectroscopy

Australian Journal of Chemistry

Volumn 52, Issue 9, 1999, Pages 861-866

  Grillo, Vincent A ^a   Gahan, Laurence R ^a   Hanson, Graeme R ^a   Hambley, Trevor W ^b   Stranger, Robert ^c   Moubaraki, Boujemaa ^d   Murray, Keith S ^d  

^a UNIVERSITY OF QUEENSLAND   (Australia)

^b UNIVERSITY OF SYDNEY   (Australia)

^c AUSTRALIAN NATIONAL UNIVERSITY   (Australia)

^d MONASH UNIVERSITY   (Australia)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0006735935     PISSN: 00049425     EISSN: None     Source Type: Journal    
DOI: 10.1071/CH97084     Document Type: Article

References (47)

1. Kahn, O., Angew. Chem., Int. Ed. Engl., 1985, 24, 834.
2. Hay, P. J., Thibeault, J. C., and Hoffman, R., J. Am. Chem. Soc., 1975, 97, 4884.
3. Karlin, K., and Zubieta, J., (Eds) 'Biological & Inorganic Copper Chemistry' Vols 1,2 (Adenine Press: New York 1984).
4. Spiro, T. G., (Ed.) 'Copper Proteins' (John Wiley: New York 1981).
5. Solomon, E. I., Penfield, K. W., and Wilcox, D. E., Struct. Bonding (Berlin), 1983, 53, 1.
6. Volbeda, A., and Hol, W. G., J. Mol. Biol., 1989, 206, 531.
7. Hazes, B., Magnus, K. A., Bonaventura, C., Bonaventura, J., Dauter, Z., Kalk, K. H., and Hol, W. G., J. Biol. Sci., 1993, 2, 597.
8. Karlin, K. D., Hayes, J. C., Gultneh, Y., Cruse, R. W., McKown, J. W., Hutchinson, J. P., and Zubieta, J., J. Am. Chem. Soc., 1984, 106, 2121.
9. Blackburn, N. J., Karlin, K. D., Concannon, M., Hayes, J. C., Gultneh, Y., and Zubieta, J., J. Chem. Soc., Chem. Commun., 1984, 939.
10. Karlin, K. D., Cruse, R. W., Haka, M. S., Gultneh, Y., and Cohen, B. T., Inorg. Chim. Acta, 1986, 125, L43.
11. Kitajima, N., and Moro-oka, Y., Chem. Rev., 1994, 94, 737.
12. Lang, W. H., and van Holde, K. E., Proc. Natl Acad. Sci. U.S.A., 1991, 88, 244.
13. Gahan, L. R., Grillo, V. A., Hambley, T. W., Hanson, G. R., Hawkins, C. J., Proudfoot, E. M., Moubaraki, B., Murray, K. S., and Wang, D., Inorg. Chem., 1996, 35, 1039.
14. Gahan, L. R., Lawrance, G. A., and Sargeson, A. M., Aust. J. Chem., 1982, 35, 1119.
15. Grillo, V. A., Hanson, G. R., Hambley, T. W., Gahan, L. R., Murray, K. S., and Moubaraki, B., J. Chem. Soc., Dalton Trans., 1997, 305.
16. Clarkson, J. A., Yagbasan, R., Blower, P. J., and Cooper, S. R., J. Chem. Soc., Chem. Commun., 1989, 1244.
17. Enraf-Nonius Structure Determination Package, Enraf-Nonius, Delft, Holland, 1985.
18. Sheldrick, G. M., SHELX-86 in 'Crystallographic Computing 3' (Eds G. M. Sheldrick, C. Krüger and R. Goddard) pp. 175-189 (Oxford University Press: Oxford, U.K., 1985).
19. Sheldrick, G. M., SHELX-76, Program for Crystal Structure Determination, University of Cambridge, 1976.
20. Cromer, D. T., and Waber, J. T., 'International Tables for X-Ray Crystallography' Vol. 4 (Kynoch Press: Birmingham 1974).
21. Johnson, C. K., ORTEP, a Thermal Ellipsoid Plotting Program, Oak Ridge National Laboratory, Oak Ridge, Tennessee, 1965.
22. van den Brenk, A. L., Fairlie, D. P., Gahan, L. R., Hanson, G. R., Hawkins, C. J., and Jones, A., Inorg. Chem., 1994, 33, 2280.
23. Karlin, K. D., Haka, M. S., Cruse, R. W., Meyer, G. J., Farooq, A., Gultneh, Y., Hayes, J.C., and Zubieta, J., J. Am. Chem. Soc., 1988, 110, 1196.
24. Jacobson, R. R., Tyeklar, Z., Farooq, A., Karlin, K. D., Liu, S., and Zubieta, J., J. Am. Chem. Soc., 1988, 110, 3690.
25. Sanyal, I., Mahroof-Tahir, M., Nasir, M. S., Ghosh, P., Cohen, B. I., Gultneh, Y., Cruse, R. W., Farooq, A., Karlin, K. D., Liu, S., and Zubieta, J., Inorg. Chem., 1992, 31, 4322.
26. Nasir, M. S., Cohen, B. I., and Karlin, K. D., J. Am: Chem. Soc., 1992, 114, 2482.
27. Kitajima, N., Fujisawa, K., Fujimoto, C., Moro-oko, Y., Hashimoto, S., Kitagawa, T., Toriumi, K., Tatsumi, K., and Nakamura, A., J. Am. Chem. Soc., 1992, 114, 1277.
28. Crawford, V. H., Richardson, H. W., Wasson, J. R., Hodgson, D. J., and Hatfield, W. E., Inorg. Chem., 1976, 15, 2107.
29. Chaudhuri, P., Ventur, D., Wieghardt, K., Peters, E.-M., Peters, K., and Simon, A., Angew. Chem., Int. Ed. Engl., 1985, 24, 57.
30. Setzer, W. N., Ogle, C. A:, Wilson, G. S., and Glass; R. S., Inorg. Chem., 1983, 22, 260.
31. Gahan, L. R., Kennard, G. H. L., Smith, G., and Mak, T. C. W., Transition Met. Chem., 1986, 11, 465.
32. Boeyens, J. C. A., Dobson, S. M., and Hancock, R. D., Inorg., Chem., 1985, 24, 3073.
33. Castro, I., Julve, M., De Munno, G., Bruno, G., Real, J. A., Lloret, F., and Faus, J., J. Chem. Soc., Dalton Trans., 1992, 1739.
34. O'Connor, C. J., Prog. Inorg. Chem., 1982, 29, 203.
35. Mann, K. L. V., Jeffery, J. C., McCleverty, J. A., Thornton, P., and Ward, M. D., J. Chem. Soc., Dalton Trans., 1998, 89.
36. Ruiz, E., Alemany, P., Alvarez, S., and Cano, J., J. Am. Chem. Soc., 1997, 119, 1297.
37. Volkov, V. V., Rakitin, Y. V., and Kalinnikov, V. T., Koord Khim., 1983, 9, 31.
38. Birker, P. J. M. W. L., Helder, J., Henkel, G., Krebs, B., and Reedijk, J., Inorg. Chem., 1982, 21, 357.
39. Banci, L., Bencini, A., and Gatteschi, D., J. Am. Chem. Soc., 1983, 105, 761.
40. Villa, J. F., and Hatfield, W. E., Inorg. Chim. Acta. 1971, 5, 145.
41. Peisach, J., and Blumberg, W. E., Arch. Biochem. Biophys., 1914, 165, 691.
42. Lever, A. P. B., 'Inorganic Spectroscopy' 2nd Edn (Elsevier: Amsterdam 1984).
43. Dagdigian, J. V., McKee, V., and Reed, C. A., Inorg. Chem., 1982, 21, 1332.
44. Amundsen, A. R., Whelan, J., and Bosnich, B., J. Am. Chem. Soc., 1977, 99, 6730.
45. Ferris, N. S., Woodruff, W. H., Rorabacher, D. B., Jones, T. E., and Ochrymowycz, L. A., J. Am. Chem. Soc., 1978, 100, 5939.
46. McMillian, D. R., and Morris, M. C., Proc. Natl Acad. Sci. U.S.A., 1981, 78, 6567.
47. Miskowski, V. M., Thich, J. A., Solomon, R., and Schugar, H. J., J. Am. Chem. Soc., 1976, 98, 8344.