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The use of Chemical Abstracts Service names has been attempted throughout this paper.
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Due to their instability on silica gel, upon isolation of the acetals a small amount impurity was always obtained. Correct elemental analyses could not be obtained from 16 and 22.
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The deep red color of the hydroxy carbene solution immediately changed to yellow, the color of the tetramethylammonium salt, upon addition of the amine.
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1H FT-NMR Spectra # 1,1033 C, and The Aldrich Library of FT-IR Spectra # 1, 659 B.
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The formation of a pink suspension in place of a faint yellow solution was observed in all cases where an acetal was formed. Upon addition of water, the suspension dissolves and changes color producing a light green aqueous phase.
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From chromium hexacarbonyl and sec-butyllithium followed by treatment of the intermediate lithium salt with tetramethylammonium chloride as described by Fischer and Maasböl in ref 17g.
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