Determination of hydrogen sulfide in blood by gas chromatography/mass spectrometry after liquid-liquid-solid phase-transfer-catalyzed pentafluorobenzylation

Japanese Journal of Forensic Toxicology

Volumn 17, Issue 1, 1999, Pages 14-21

  Miki, Akihiro ^a   Tsuchihashi, Hitoshi ^a  

^a Chuo ward   (Japan)

Author keywords

Blood; GC MS; Hydrogen sulfide; Pentafluoro benzylation; Phase transfer catalysis; Sulfide

Indexed keywords

EID: 0006032138     PISSN: 09159606     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (12)

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8. Starks, C. M., Liotta, C. L. and Halpern, M.: Phase-Transfer Catalysis, Fundamentals, Applications, and Industrial Perspectives, Chapman & Hall, London, 1994.
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10. Keller, W. E.: Fluka-Compendium on Phase-Transfer Reactions, Vol. 3, Georg Thieme Verlag, New York, 1992.
11. Miki, A., Tsuchihashi, H., Ueda, K., Yamano, H. and Yamashita, M.: Gas chromatographic and gas chromatography/mass spectrometric determination of aqueous poisons via extractive pentafluorobenzylation using a polymeric phase transfer catalyst. Proceedings of the 30th international meeting of the International Association of Forensic Toxicologists, Fukuoka, 1992, pp. 419-424.
12. Kage, S.: Determination of sulfide, thiosulfide and polysulfide in biological materials by GC-ECD and GC/MS. Jpn J Forensic Toxicol, 16, 128-131 (1998).