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note
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-3. Intensity data were collected using Rigaku-AFC5R automated four-circle diffractometer with graphite monochro-mated Mo-Kα radiation (λ=0.71073 Å). 2396 independent reflections (I>3σ(I)) were used for the structure analysis. The crystal structure was solved by the direct method (SHELX86) and refined by a full-matrix least squares method . Final R and Rw values were 0.046 and 0.028, respectively.
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