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Tetrahedron Letters
Volumn 13, Issue 9, 1972, Pages 791-794
A new synthetic route to the fungal sex hormone antheridiol and the determination of its absolute stereochemistry
Author keywords

[No Author keywords available]
Indexed keywords

EID: 0004597556     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(01)84440-3     Document Type: Article
Times cited : (19)
References (14)
  • 3
    • 84914378924 scopus 로고    scopus 로고
    • 3), 1.68 (m, J 7 Hz, methine H), 3.85 and 4.42 ppm (2 × d, J 2 Hz, furyl-H)]. Since the bromofuran distillate gradually darkened during the course of the distillation, the dried steam distillate was treated directly with n-butyl-lithium in hexane to form the lithio derivative.
  • 5
    • 84914378923 scopus 로고    scopus 로고
    • Satisfactory elemental analyses were obtained for all fully characterized compounds.
  • 6
    • 85004280914 scopus 로고
    • Studies on Digitalis Glycosides. XXXII. Condensation of 17β-(3-Furyl)-5β, 14β-androstane-3β, 14, 16β-triol with Carbonyl Compounds
    • During the course of this work, described the conversion of a 17β-furylandrostane to an α,β-unsaturated lactone by the same sequence of reactions.
    • (1970) CHEMICAL & PHARMACEUTICAL BULLETIN , vol.18 , pp. 1239
    • Satoh1    Auyama2
  • 9
    • 84914378922 scopus 로고    scopus 로고
    • In our first synthesis of antheridiol 1, lactone 9a was not isolated in a pure state. Antheridiol was obtained by treating γ-lactone fraction rich in 9a by the zinc reduction and photoxygenation procedures. See ref. 4.
  • 10
    • 0039404216 scopus 로고
    • 4 followed by acid hydrolysis. This furnished, among other products, the butenolides 9b and 9c in low yield. Unpublished results of W. Salmond from these laboratories.See also
    • (1971) J. Chem. Soc. , vol.500 , pp. 1646
    • McMorris1    Seshadri2

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.