An ex situ methodology for characterization of coke by TGA and 13C CP-MAS NMR spectroscopy

Applied Catalysis A: General

Volumn 165, Issue 1-2, 1997, Pages 489-497

  Pradhan, A R ^a   Wu, J F ^a   Jong, S J ^a   Tsai, T C ^b   Liu, S B ^a  

^a INSTITUTE OF ATOMIC AND MOLECULAR SCIENCES   (Taiwan)

^b CPC CORPORATION   (Taiwan)

Author keywords

13c ; Coke; Cracking; Disproportionation; NMR spectroscopy; Thermogravimetric analysis; Zeolite

Indexed keywords

EID: 0003894908     PISSN: 0926860X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0926-860X(97)00231-7     Document Type: Article

References (30)

1. M. Guisnet, P. Magnoux, Appl. Catal. 54 (1989) 1.
2. S. Bhatia, J. Beltramini, D.D. Do, Catal. Rev.-Sci. Eng., 31 (1989-1990) 431.
3. H.G. Karge, Stud. Surf. Sci. Catal. 58 (1991) 531.
4. D.M. Bibby, R.F. Howe, G.D. McLellan, Appl. Catal. A: General 93 (1992) 1.
5. M. Guisnet, P. Magnoux, Stud. Surf. Sci. Catal. 88 (1994) 53.
6. J.R. Anderson, Y.-F. Chang, R.J. Western, J. Catal. 118 (1989) 466.
7. N.Y. Chen, W.E. Garwood, F.G. Dwyer, Shape Selective Catalysis in Industrial Applications, (Chem. Ind. Ser., Vol. 36), Dekker, New York, 1989.
8. J.L. Bonardet, M.C. Barrage, J. Fraissard, J. Mol. Catal. A 96 (1995) 123.
9. J.F. Haw, in A.T. Bell, A. Pines (Editors), NMR Techniques in Catalysis, Marcel and Dekker, New York, 1994, ch. 3.
10. M. Stocker, Stud. Surf. Sci. Catal. 85 (1994) 429.
11. I.I. Ivanova, E.G. Derouane, Stud. Surf. Sci. Catal. 85 (1994) 357.
12. S.B. Liu, S. Prasad, J.F. Wu, L.J. Ma, T.C. Yang, J.T. Chiou, J.Y. Chang, T.C. Tsai, J. Catal. 142 (1993) 664.
13. W.H. Chen, A.R. Pradhan, S.J. long, T.Y. Lee, I. Wang, T.C. Tsai, S.B. Liu, J. Catal. 163 (1996) 436.
14. E.R. Andrew, A. Bradbury, R.G. Eades, Nature (London) 182 (1958) 1659.
15. I.J. Lowe, Phys. Rev. Lett. 2 (1959) 285.
16. A. Pines, M.G. Gibby, J.S. Waugh, J. Chem. Phys. 56 (1972) 1776.
17. C.A. Fyfe, Solid State NMR for Chemists, C.F.C. Press, Ontario, 1983.
18. G. Engelhardt, D. Michel, High-Resolution Solid-State NMR of Silicates and Zeolites, Wiley, New York, 1987.
19. J.P. Lange, A. Gutsze, J. Allgeier, H.G. Karge, Appl. Catal. 45 (1988) 345.
20. M.W. Anderson, J. Klinowski, Nature 339 (1989) 200.
21. J.F. Haw, B.R. Richardson, I.S. Oshiro, N.D. Lazo, J.A. Speed, J. Am. Chem. Soc. 111 (1989) 2052.
22. M.W. Anderson, J. Klinowski, J. Am. Chem. Soc. 112 (1990) 10.
23. A.G. Stepanov, K.I. Zamaraev, J.M. Thomas, Catal Lett. 13 (1992) 407.
24. I.I. Ivanova, D. Brunel, G. Daelen, J.B. Nagy, E.G. Derouane, Stud. Surf. Sci. Catal. 78 (1993) 587.
25. A. Philippou, M.W. Anderson, J. Catal. 158 (1996) 385.
26. I.I. Ivanova, A. Pasau-Claerbout, M. Seirvert, N. Blam, E.G. Derouane, J. Catal. 158 (1996) 521.
27. A.R. Pradhan, W.H. Chen, J.F. Wu, S.J. Jong, T.C. Tsai, S.B. Liu, Appl. Catal, in press (1997).
28. J.B. Stothers, Carbon-13 NMR Spectroscopy, Academic Press, New York, 1972.
29. R.M. Silverstein, G.C. Bassler, T.C. Morvill, Spectroscopic Investigation of Organic Compounds, New York, 1991, ch. 5.
30. E. Breitmaier, G. Haas, W. Voelter, Atlas of Carbon-13 NMR Data, Heyden and Son, London, 1979.