메뉴 건너뛰기




Volumn 36, Issue 18, 1997, Pages 3806-3807

Synthesis and Characterization of Two New Telluroindates: K6In2Te64C2H8N 2and (Ph4P)2In2Te6

Author keywords

[No Author keywords available]

Indexed keywords


EID: 0003282667     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic9702882     Document Type: Article
Times cited : (26)

References (33)
  • 22
    • 2442668197 scopus 로고    scopus 로고
    • note
    • -1, crystal dimension 0.23 × 0.20 × 0.10 mm, R = 0.031, R = 0.031. The data were collecled (+h.+k.+l) at 293 K on a Rigaku AFC7R four-circle diffractometer equipped with a RU300 18KW rotating anode, in the range of 20 < 40° using a -2 scan at a scan rate of 8 deg/min. A total of 1973 reflections were measured, of which 1637 reflections with 1 > 3(1) were considered as observed. An empirical absorption correction using the program DIFABS was applied (transmission 1.000-0.811). The structure was solved by direct methods and refined by the teXsan crystallographic software package of Molecular Structure Corp. All atoms were refined anisotropically except H atoms were fixed. Oneof nitrogen atoms in ethylenediamine was refined with a disordered model.
  • 27
    • 2442709443 scopus 로고    scopus 로고
    • note
    • -1, crystal dimension 0.20 × 0.04 ×0.02 mm R = 0.062. R, = 0.065. The data were collected (+h,+k,-l) at 293 K on a Rigaku AFC7R four-circle diffractometer equipped with a RU300 18KW rotating anode, in the range of 20 < 40° using a scan at a scan rate of 4 deg/min. A total of 1388 reflections were measured, of which 676 reflections with 1 > >3(1) were considered as observed. An empirical absorption correction was applied (transmission 1.0000.559). The structure was solved by direct methods and refined by the teXsan crystallographic software package of Molecular Structure Corp. In. Te, and P atoms were refined anisotropically, and carbon atoms were refined isotropically and mostly fixed. One phenyl ring was refined with a disordered model.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.