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44
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0000793212
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Obtained from the imidazolium salt by deprotonation as described in: A. J. Arduengo, J. Am. Chem Soc 1992, 114, 5530-5534.
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(1992)
J. Am. Chem Soc
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Arduengo, A.J.1
-
45
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0001634009
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-
W. A. Herrmann, M. Denk, J. Behm, W. Scherer, F.-R. Klingan, H Bock, B. Solouki, M. Wagner, Angew. Chem. 1992, 104, 1489-1492; Angew. Chem. Int. Ed. Engl. 1992, 31, 1485-1488.
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Herrmann, W.A.1
Denk, M.2
Behm, J.3
Scherer, W.4
Klingan, F.-R.5
Bock, H.6
Solouki, B.7
Wagner, M.8
-
46
-
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33745344889
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-
W. A. Herrmann, M. Denk, J. Behm, W. Scherer, F.-R. Klingan, H Bock, B. Solouki, M. Wagner, Angew. Chem. 1992, 104, 1489-1492; Angew. Chem. Int. Ed. Engl. 1992, 31, 1485-1488.
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Angew. Chem. Int. Ed. Engl.
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-
-
-
47
-
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85163231427
-
-
note
-
-1: 3107 w, 1639 m, 1598 m, 1393 m, 1368 s, 1343 m, 1270 s, 1212 s, 1196 s, 1122 s, 1106 s, 1089 s, 1048 s, 999 s, 810 m, 744 s, 663 s, 647 s.
-
-
-
-
48
-
-
85163223551
-
-
note
-
3.
-
-
-
-
49
-
-
85163223771
-
-
note
-
1H NMR). The NMR tubes were stored "upside down" during the thermolysis to prevent the formation of a tin film in the bottom part of the NMR tube.
-
-
-
-
50
-
-
85163223849
-
-
note
-
2 and tin powder as sole products.
-
-
-
-
51
-
-
85163233072
-
-
unpublished results
-
+•, 195 (5), 158 (9), 156 (7), 156 (41), 155 (12), 154 (62), 153 (7), 140 (21), 133 (3), 125 (16), 121 (32), 120 (12), 119 (87), 99 (5), 94 (4), 92 (10), 85 (14), 84 (53), 83 (3), 57 (8). The identity of the compound has also been confirmed by single crystal X-ray diffraction (M. Denk, unpublished results).
-
-
-
Denk, M.1
-
54
-
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84885434331
-
-
Siemens Analytical X-ray Instruments Inc., Madison, Wisconsin, U. S. A.
-
Sheldrick, G. M., SHELXTL\PC, Siemens Analytical X-ray Instruments Inc., Madison, Wisconsin, U. S. A. (1994).
-
(1994)
SHELXTL\PC
-
-
Sheldrick, G.M.1
-
55
-
-
85163224679
-
-
note
-
Crystallographic data (excluding structure factors) for the structure of 5 have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-101272. Copies of the data can be obtained free of charge on applications to the Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: Int. Code +44(0)1223/ 336-033. E-mail: deposit@chemcrys.cam.ac.uk).
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