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Volumn , Issue 8, 1998, Pages 1067-1070

Reaction of a Stable Silylene with Divalent Group 14 Compounds

Author keywords

Carbene analogs; N Heterocycles; Silylene; Subvalent compounds; Tin

Indexed keywords

DEPOSITION; ORGANIC COMPOUNDS; PHOTOLYSIS; POLYSILANES; PYROLYSIS; SINGLE CRYSTALS; THERMOLYSIS; TIN COMPOUNDS; X RAY DIFFRACTION;

EID: 0003088929     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1099-0682(199808)1998:8<1067::AID-EJIC1067>3.0.CO;2-7     Document Type: Article
Times cited : (38)

References (55)
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    • note
    • -1: 3107 w, 1639 m, 1598 m, 1393 m, 1368 s, 1343 m, 1270 s, 1212 s, 1196 s, 1122 s, 1106 s, 1089 s, 1048 s, 999 s, 810 m, 744 s, 663 s, 647 s.
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    • 3.
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    • note
    • 1H NMR). The NMR tubes were stored "upside down" during the thermolysis to prevent the formation of a tin film in the bottom part of the NMR tube.
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    • note
    • 2 and tin powder as sole products.
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    • unpublished results
    • +•, 195 (5), 158 (9), 156 (7), 156 (41), 155 (12), 154 (62), 153 (7), 140 (21), 133 (3), 125 (16), 121 (32), 120 (12), 119 (87), 99 (5), 94 (4), 92 (10), 85 (14), 84 (53), 83 (3), 57 (8). The identity of the compound has also been confirmed by single crystal X-ray diffraction (M. Denk, unpublished results).
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    • note
    • Crystallographic data (excluding structure factors) for the structure of 5 have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-101272. Copies of the data can be obtained free of charge on applications to the Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: Int. Code +44(0)1223/ 336-033. E-mail: deposit@chemcrys.cam.ac.uk).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.