Hydrothermal synthesis and characterization of a new vanadyl sulfate compound: Crystal structure of [V(IV)OSO4(H2O)4]·SO 4·[H2N(C2H4) 2NH2]

Inorganica Chimica Acta

Volumn 292, Issue 1, 1999, Pages 112-116

  Khan, M Ishaque ^a   Cevik, Sabri ^a   Doedens, Robert J ^b  

^a Illinois Eye Inst   (United States)

^b UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

Crystal structures; Hydrothermal synthesis; Vanadyl sulfate

Indexed keywords

CRYSTAL STRUCTURE; ETHYLENE; HYDROGEN BONDS; INORGANIC COMPOUNDS; LEAST SQUARES APPROXIMATIONS; SODIUM SULFATE; SULFUR COMPOUNDS; VANADIUM COMPOUNDS;

DIRECT METHOD; HYDROTHERMAL REACTION; LEAST SQUARES REFINEMENT; ORGANIC SPECIES; ORGANIC-INORGANIC COMPOUND; SYNTHESIS AND CHARACTERIZATIONS; VANADYL ACETYLACETONATE; VANADYL SULFATE;

HYDROTHERMAL SYNTHESIS;

EID: 0003043204     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0020-1693(99)00153-X     Document Type: Article

References (27)

1. (a) R.C. Haushalter, L. Mundi, Chem. Mater. 4 (1992) 31.
2. (b) J. Zubieta, Comments Inorg. Chem. 16 (1994) 153, and references therein.
3. (c) R.C. Haushalter, L.M. Meyer, J. Zubieta, in: M.H. Chisholm (Ed.), Early Transition Metal Clusters With Π-Donor Ligands, VCH, New York, 1995.
4. (d) E. Canadell, J. Provost, A. Guesdon, M.M. Borel, A. Leclaire, Chem. Mater. 9 (1997) 68.
5. (e) R.C. Haushalter, K. Strohmaier, F. Lai, Science 246 (1989) 1289.
6. (f) J. Chen, R. Jones, S. Natarajan, M.B. Hursthouse, J.M. Thomas, Angew. Chem., Int. Ed. Engl. 33 (1994) 639.
7. (g) M.I. Khan, L.M. Meyer, R. Haushalter, J. Zubieta, A. Schweitzer, J.L. Dye, Chem. Mater. 8 (1996) 43.
8. (a) K.M. Eriksen, K. Nielsen, R. Fehrmann, Inorg. Chem. 35 (1996) 480, and references therein.
9. (b) K. Nielson, R. Fehrmann, K.M. Eriksen, Inorg. Chem. 32 (1993) 4825.
10. (a) K.-L. Richter, R. Mattes, Inorg. Chem. 30 (1991) 4367, and references therein.
11. (b) K.-W. Richter, R. Mattes, Z. Anorg. Allg. Chem. 611 (1992) 158.
12. (a) Y.-D. Chang, Q. Chen, M.I. Khan, J. Salta, J. Zubieta, J. Chem. Soc., Chem. Commun. (1993) 1872.
13. (b) L.M. Daniels, C.A. Murrilo, K.G. Rodriguez, Inorg. Chim. Acta 229 (1995) 27.
14. (a) G.D. Munno, C. Bazzicalupi, J. Faus, F. Lloret, M. Julve, J. Chem. Soc., Chem. Commun. (1994) 1879.
15. (b) L. Heerman, H.V. Nyen, W. D'Olieslager, Inorg. Chim. Acta 244 (1996) 191.
16. Khan M.I., Cevik S., Powell D., Li S., O'Connor C.J. Inorg. Chem. 37:1998;81.
17. Lazoryak B.I. Russ. Chem. Rev. 65:1996;287.
18. Ballhausen C.J., Djurinskij B.F., Watson K.J. J. Am. Chem. Soc. 90:1968;3305.
19. Longo J.M., Arnott R.J. J. Solid State Chem. 1:1970;394. and references therein.
20. SMART, Version 4.210, Siemens Analytical X-Ray Systems, Madison, WI, 1997.
21. SAINT, Version 4.050, Siemens Analytical X-Ray Systems, Madison, WI, 1995.
22. G.M. Sheldrick, SADABS, University of Göttingen, Germany, 1997.
23. G.M. Sheldrick, SHELXTL Version 5.03, Siemens Industrial Automation, Madison, WI, 1995.
24. I.D. Brown, in: M. O'Keefe, A. Navrotsky (Eds.), Structure and Bonding in Crystals, vol. II, Academic Press, New York, 1981, p. 1.
25. B.R. Nechay, Ann. Rev. Pharm. Toxicol. 24 (1984) 501.
26. (a) Y. Shechter, S.J.D. Karlish, Nature (London) 284 (1980) 556.
27. (b) M. Nakai, H. Watanabe, C. Fujiwara, H. Kakegawa, T. Satoh, J. Takada, R. Matsushita, H. Sakurai, Biol. Pharm. Bull. 18 (1995) 719, and references therein.