Diene Complexes of trans-5-Palladatricyclo[4.1.0.02,4]heptanes

European Journal of Inorganic Chemistry

Volumn , Issue 12, 1998, Pages 1987-1990

  Hashmi, A Stephen K ^a   Bats, Jan W ^a   Naumann, Frank ^a   Berger, Bernd ^a  

^a GOETHE UNIVERSITY   (Germany)

Author keywords

Diene complexes; Metallacycles; Palladium

Indexed keywords

OLEFINS; PALLADIUM COMPOUNDS;

CARBON BOND; DIENE COMPLEX; METALLACYCLES; N-O COMPLEXES; NORBORNADIENE; X-RAY STRUCTURE DETERMINATIONS;

HEPTANE;

EID: 0002909009     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1099-0682(199812)1998:12<1987::AID-EJIC1987>3.0.CO;2-6     Document Type: Article

References (36)

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12. Crystallographic data (excluding structure factors) for rac-5 and rac-6 have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no CCDC-102022 (rac-5) and -102023 (rac-6). Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [Fax: (internat.) + 44(0)1223/336033; E-mail: deposit@ccdc.cam.ac.uk].
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15. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
16. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
17. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
18. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
19. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
20. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
21. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
22. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
23. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
24. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
25. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
26. 4-1,5-cyclooctadiene)palladmm(II), is known: N. C. Baenziger, C. V. Goebel, T. Berg, J. R. Doyle, Acta Crystallogr., Sect. B 1978, 34, 1340-1342. In all other structures such a twist-boat-like conformation was observed: L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. M. F. Rettig, R. M. Wing, G. R. Wiger, J. Am. Chem. Soc. 1981, 103, 2980-2986. R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle. N. C. Baenziger, M. A. M. Howells, Acta Crystallogr., Sect. C 1993, 49, 1766-1767. D. E. Smith, A. J. Welch, Acta Crystallogr., Sect. C 1986, 42, 1717-1720. J. Vicente, I. Saura-Llamas, P. G. Jones, J. Chem. Soc, Dalton Trans. 1993, 3619-3624. L. Benchekroun, P. Herpin, M. Julia, L. Saussine, J. Organomet. Chem. 1977, 128, 275-290. R. M. Buchanan, C. G. Pierpont, Inorg. Chem 1979, 18, 3608-3610. A. C. Albeniz, P. Espinet, Y. Jeannin, M. Piloche-Levisalles, B. E. Mann, J. Am. Chem. Soc. 1990, 112, 6594-6600. P. Stepnicka, I. Cisarova, Collect. Czech Chem. Commun. 1996, 61, 1335-1341. N. L. Douek, A. J. Welch, J. Chem Soc., Dalton Trans. 1993, 1917-1925, K. A. Fallis, D. F. Mullica, E. L. Sappenfield, F. G. A. Stone, Inorg. Chem. 1994, 33, 4927-4933. I. R. Butler, M. Kalaji, L. Nehrlich, M. Hursthouse, A. I. Kataulov, K. M. A. Malik, J. Chem. Soc., Chem. Comm. 1995, 459-460.
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