Synthesis and structure of [Bi2(NtBu)4]2Li 2·2THF; a bimetallic cubane fragment containing a [Bi2(NtBu)4]2- anion

Inorganica Chimica Acta

Volumn 248, Issue 1, 1996, Pages 9-14

  Edwards, Andrew J ^a   Beswick, Michael A ^a   Galsworthy, Jane R ^a   Paver, Michael A ^a   Raithby, Paul R ^a   Rennie, Moira Ann ^a   Russell, Christopher A ^a   Verhorevoort, Kerry L ^a   Wright, Dominic S ^a  

^a UNIVERSITY OF CAMBRIDGE   (United Kingdom)

Author keywords

Bismuth complexes; Crystal structures; Cubane complexes; Imido complexes

Indexed keywords

CRYSTAL STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; TEMPERATURE;

1H NMR SPECTROSCOPY; BISMUTH COMPLEXES; CUBANE COMPLEXES; IMIDO COMPLEXES; IN-SITU REACTIONS; LOW TEMPERATURES; MONOCLINIC SPACE GROUPS; X-RAY DIFFRACTION STUDIES;

BISMUTH COMPOUNDS;

EID: 0002872958     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/0020-1693(95)04974-6     Document Type: Article

References (39)

1. (a) A.J. Edwards, N.E. Leadbeater, M.A. Paver, P.R. Raithby, C.A. Russell and D.S. Wright, J. Chem. Soc., Dalton Trans., (1994) 1479;
2. (b) A.J. Edwards, M.A. Paver, M.-A. Rennie, C.A. Russell, P.R. Raithby and D.S. Wright, J. Chem. Soc., Dalton Trans., (1994) 2963.
3. A.J. Edwards, P. Pearson, M.A. Paver, P.R. Raithby, M.-A. Rennie, C.A. Russell and D.S. Wright, J. Organomet. Chem., 503 (1995) C29.
4. (a) R.A. Alton, D. Barr, A.J. Edwards, M.A. Paver, P.R. Raithby, M.-A. Rennie, C.A. Russell and D.S. Wright, J. Chem. Soc., Chem. Commun., (1994) 1481;
5. (b) A.J. Edwards, M.A. Paver, P.R. Raithby, M.-A. Renie, C.A. Russel and D.S. Wright, Angew. Chem., 106 (1994) 1334; Angew. Chem., Int. Ed. Engl., 33 (1994) 1277.
6. (b) A.J. Edwards, M.A. Paver, P.R. Raithby, M.-A. Renie, C.A. Russel and D.S. Wright, Angew. Chem., 106 (1994) 1334; Angew. Chem., Int. Ed. Engl., 33 (1994) 1277.
7. (a) D. Barr, A.J. Edwards, S. Pullen, M.A. Paver, M.-A. Rennie, P.R. Raithby, C.A. Russell and D.S. Wright, Angew. Chem., 106 (1994) 1960; Angew. Chem., Int. Ed. Engl., 33 (1994) 1875;
8. (a) D. Barr, A.J. Edwards, S. Pullen, M.A. Paver, M.-A. Rennie, P.R. Raithby, C.A. Russell and D.S. Wright, Angew. Chem., 106 (1994) 1960; Angew. Chem., Int. Ed. Engl., 33 (1994) 1875;
9. (b) D. Barr, A.J. Edwards, M.A. Paver, P.R. Raithby, M.-A. Rennie, C.A. Russel and D.S. Wright, Angew. Chem., 107 (1995) 1088; Angew. Chem., Int. Ed. Engl., 34 (1995) 1012.
10. (b) D. Barr, A.J. Edwards, M.A. Paver, P.R. Raithby, M.-A. Rennie, C.A. Russel and D.S. Wright, Angew. Chem., 107 (1995) 1088; Angew. Chem., Int. Ed. Engl., 34 (1995) 1012.
11. D.F. Shriver and M.A. Drezdon, The Manipulation of Air-Sensitive Compounds, Wiley, New York, 2nd edn., 1986.
12. M.G. Davidson, R. Snaith, D. Stalke and D.S. Wright, J. Org. Chem., 38 (1993) 2810.
13. (a) F. Ando, T. Hayashi, K. Ohashi and J. Koketsu, J. Inorg. Nucl. Chem., 37 (1975) 2011;
14. (b) W. Clegg, N.A. Compton, R.J. Errington, G.A. Fischer, M.E. Green, D.R. Hockless and N.C. Norman, Inorg. Chem., 30 (1991) 4680.
15. (a) K. Moedritzer, Inorg. Chem., 3 (1964) 609;
16. (b) A. Kiennemann, G. Levy, F. Schué and J. Taniélian, J. Organomet. Chem., 35 (1972) 143.
17. T. Kottke and D. Stalke, J. Appl. Crystallogr., 26 (1993) 615.
18. G.M. Sheldrick, SHELXL-93, University of Göttingen, Germany, 1993.
19. (a) P. Hornig, O.J. Scherer and M. Schmidt, J. Organomet. Chem., 6 (1966) 259;
20. (b) W. Clegg, N.A. Compton, J. Errington, N.C. Norman and N. Wishart, Polyhedron, 8 (1989) 1579.
21. M. Noltemeyer, H.W. Roesky, H. Schmidt and U. Wirringa, Inorg. Chem., 33 (1994) 4607.
22. (a) R.E. Mulvey, Chem. Soc. Rev., 20 (1991) 167;
23. (b) K. Gregory, P.v.R. Schleyer and R. Snaith, Adv. Inorg. Chem., 37 (1991) 47.
24. G. Del Piero, M. Cesari, G. Perego, S. Cucinella and E. Cernia, J. Organomet. Chem., 129 (1977) 289.
25. S. Amirkhalili, P.B. Hitchcock and J.D. Smith, J. Chem. Soc., Dalton Trans., (1979) 1206.
26. (a) L. Zsolnai, G. Huttner and M. Driess, Angew. Chem., 105 (1993) 1549; Angew. Chem., Int. Ed. Engl., 32 (1993) 1439;
27. (a) L. Zsolnai, G. Huttner and M. Driess, Angew. Chem., 105 (1993) 1549; Angew. Chem., Int. Ed. Engl., 32 (1993) 1439;
28. (b) D.J. Brauer, H. Bürger, G.L. Liewald and J. Wilke, J. Organomet. Chem., 287 (1985) 305;
29. (c) D.J. Brauer, H. Bürger and G.L. Liewald, J. Organomet. Chem., 308 (1986) 119;
30. (d) M. Veith, A. Spaniol, J. Pöhlmann, F. Gross and V. Huch, Chem. Ber., 126 (1993) 2625;
31. (e) O.J. Scherer, G. Wolmershäuser and H. Conrad, Angew. Chem., 95 (1983) 427; Angew. Chem., Int. Ed. Engl., 22 (1983) 404;
32. (e) O.J. Scherer, G. Wolmershäuser and H. Conrad, Angew. Chem., 95 (1983) 427; Angew. Chem., Int. Ed. Engl., 22 (1983) 404;
33. (f) W. Neubert, H. Pritzkow and H.P. Latscha, Angew. Chem., 100 (1988) 298; Angew. Chem., Int. Ed. Engl., 27 (1988) 287;
34. (f) W. Neubert, H. Pritzkow and H.P. Latscha, Angew. Chem., 100 (1988) 298; Angew. Chem., Int. Ed. Engl., 27 (1988) 287;
35. (g) M. Björgvinsson, H. W. Roesky, F. Pauer and G.M. Sheldrick, Chem. Ber., 125 (1992) 767;
36. (h) M. Veith, Chem. Rev., 90 (1990) 3;
37. (i) M. Veith, F. Goffing and V. Huch, Chem. Ber., 121 (1988) 943;
38. (j) M. Rhiel, F. Weller, J. Pebler and K. Dehniche, Angew. Chem., 106 (1994) 599; Angew. Chem., Int. Ed. Engl., 33 (1994) 569.
39. (j) M. Rhiel, F. Weller, J. Pebler and K. Dehniche, Angew. Chem., 106 (1994) 599; Angew. Chem., Int. Ed. Engl., 33 (1994) 569.