Non-ionic Ln(III) chelates as MRI contrast agents: Synthesis, charactetisation and 1H NMR relaxometric investigations of bis(benzylamide)diethylenetriaminepentaacetic acid Lu(III) and Gd(III) complexes

Inorganica Chimica Acta

Volumn 254, Issue 1, 1997, Pages 63-70

  Aime, Silvio ^a   Benetollo, Franco ^b   Bombieri, Gabriella ^c   Colla, Susanna ^a   Fasano, Mauro ^a   Paoletti, Silvia ^a  

^a UNIVERSITY OF TURIN   (Italy)

^b CNR   (Italy)

^c UNIVERSITY OF MILAN   (Italy)

Author keywords

Chelate ligand complexes; Crystal structures; Lanthanide complexes; Magnetic resonance imaging; Nuclear magnetic resonance; Relaxometry

Indexed keywords

CARBOXYLATION; CHELATION; COMPLEXATION; CRYSTAL STRUCTURE; CYCLODEXTRINS; ISOMERS; LIGANDS; LUTETIUM COMPOUNDS; MAGNETIC RESONANCE IMAGING; MOLECULES; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SINGLE CRYSTALS; SYNTHESIS (CHEMICAL); THERMODYNAMIC STABILITY;

CHELATE LIGANDS; COORDINATE GEOMETRY; DIETHYLENETRIAMINE PENTA-ACETIC ACIDS; LANTHANIDE COMPLEX; MRI CONTRAST AGENTS; RELAXOMETRY; SINGLE-CRYSTAL X-RAY DIFFRACTION STUDIES; SOLID-STATE STRUCTURES;

GADOLINIUM COMPOUNDS;

EID: 0002814236     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/s0020-1693(96)05139-0     Document Type: Article

References (25)

1. R.B. Lauffer, Chem. Rev., 87 (1987) 901.
2. B.L. Engelstad and G.L. Wolf, in D.D. Stark and W.G. Bradley (eds.), Magnetic Resonance Imaging, Mosby, St. Louis, 1988, p. 161.
3. L. Ehnebom and B.F. Pedersen, Acta Chem. Scand., 46 (1992) 126.
4. K. Kumar and M.F. Tweedle, Pure Appl. Chem., 65 (1993) 515.
5. C.F.G.C. Geraldes, A.M. Urbano, M.C. Alpoim, A.D. Sherry, K.-T. Kuan, R. Rajagopalan, F. Maton and R.N. Muller, Magn. Reson. Imag., 13 (1995) 401.
6. S. Aime, M. Botta, W. Dastrù, M. Fasano, M. Panero and A. Arnelli, Inorg. Chem., 32 (1993) 2068.
7. A.D. Sherry, W.P. Cacheris and K.T. Kuan. Magn. Reson. Med., 8 (1988) 180.
8. C. Paul-Roth and K.N. Raymond, Inorg. Chem., 34 (1995) 1408.
9. L. Ehnebom, B.F. Pedersen and J. Klaveness, Acta Chem. Scand., 47 (1993) 965.
10. D. Parker, K. Pulukkody, F.C. Smith, A. Batsanov and J.A.K. Howard, J. Chem. Soc., Dalton Trans., (1994) 689.
11. S.W. Annie Bligh, A.H.M.S. Chowdhury, M. McPartlin and I.J. Scowen, Polyhedron, 14 (1995) 567.
12. A.C.T. North, D.C. Philips and F.S. Mathews, Acta Crystallogr., Sect. A, 24 (1968) 351.
13. G.M. Sheldrick, in G.M. Sheldrick, C. Kruger and R. Goddard (eds.), Crystallographic Computing 3, Oxford University Press, Oxford, UK, 1985.
14. (a) G.M. Sheldrick, Acta Crystallogr., Sect. A, 46 (1990) 467;
15. (b) G.M. Sheldrick, Z. Dauter, K.S. Wilson, H. Hope and L.C. Sieker, Acta Crystallogr., Sect. D, 49 (1993) 18.
16. C.K. Johnson, ORTEP II, Rep. ORNL-5138, Oak Ridge National Laboratory, TN, USA, 1976.
17. S. Aime, M. Fasano, S. Paoletti and E. Terreno, Gazz. Chim. Ital., 125 (1995) 125.
18. I. Bertini and C. Luchinat, NMR of Paramagnetic Molecules in Biological Systems, Benjamin/Cummings, Menlo Park, CA, 1986.
19. J.-C.G. Bünzli and G.R. Choppin (eds.), Lanthanide Probes in Life, Chemical and Earth Sciences - Theory and Practice, Elsevier, Amsterdam, 1989.
20. F. Uggeri, S. Aime, P.L. Anelli, M. Botta, M. Brocchetta, C. de Haèn, G. Ermondi, M. Grandi and P. Paoli, Inorg. Chem., 34 (1995) 633.
21. R.D. Shannon, Acta Crystallogr. Sect. A, 32 (1967) 751.
22. W.P. Cacheris, S.C. Quay and S.M. Rocklage, Magn. Reson. Imag., 8 (1990) 467.
23. S. Aime, M. Botta, M. Fasano, S. Paoletti, P.L. Anelli, F. Uggeri and M. Virtuani, Inorg. Chem., 33 (1994) 4707.
24. J. Szejtli, J. Inclusion Phenom., 14 (1992) 25.
25. D. Duchêne, Cyclodextrins and their Industrial Uses, Edition de Santé, Paris, 1987.