A Cross Metathesis Approach towards Allyl Stannanes

Synlett

Volumn 1997, Issue 1, 1997, Pages 129-130

  Feng, Jing ^a   Schuster, Matthias ^a   Blechert, Siegfried ^a  

^a TECHNISCHE UNIVERSITÄT BERLIN   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0002608727     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-1997-692     Document Type: Article

References (16)

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2. Schmalz, H.-G. Angew. Chem. 1995, 107, 1981, Angew. Chem. Ed. Engl. 1995, 34, 1833. Koert, U. Nachr. Chem. Tech. Lab. 1995, 43, 809.
3. Schmalz, H.-G. Angew. Chem. 1995, 107, 1981, Angew. Chem. Ed. Engl. 1995, 34, 1833. Koert, U. Nachr. Chem. Tech. Lab. 1995, 43, 809.
4. Schwab, P.; France, M.B.; Ziller, J.W.; Grubbs, R.H. Angew. Chem. 1995, 107, 2179; Angew. Chem. Ed. Engl. 1995, 34, 2039. Fox, H.H.; Yap, K.B.; Robbins, J.; Cai, S.; Schrock, R.R. Inorg. Chem. 1992, 31, 2287.
5. Schwab, P.; France, M.B.; Ziller, J.W.; Grubbs, R.H. Angew. Chem. 1995, 107, 2179; Angew. Chem. Ed. Engl. 1995, 34, 2039. Fox, H.H.; Yap, K.B.; Robbins, J.; Cai, S.; Schrock, R.R. Inorg. Chem. 1992, 31, 2287.
6. Schwab, P.; France, M.B.; Ziller, J.W.; Grubbs, R.H. Angew. Chem. 1995, 107, 2179; Angew. Chem. Ed. Engl. 1995, 34, 2039. Fox, H.H.; Yap, K.B.; Robbins, J.; Cai, S.; Schrock, R.R. Inorg. Chem. 1992, 31, 2287.
7. Crowe, W.E.; Goldberg, D.R. J. Am. Chem. Soc. 1995, 117, 5162. Crowe, W. E.; Goldberg, D. R.; Zhang, Z. J. Tetrahedron Lett. 1996, 37, 2117. Finkelshtein, E.Sh., Ushakov, N.V., Portnykh, E.B. J. Mol. Catalysis 1992, 76, 133.
8. Crowe, W.E.; Goldberg, D.R. J. Am. Chem. Soc. 1995, 117, 5162. Crowe, W. E.; Goldberg, D. R.; Zhang, Z. J. Tetrahedron Lett. 1996, 37, 2117. Finkelshtein, E.Sh., Ushakov, N.V., Portnykh, E.B. J. Mol. Catalysis 1992, 76, 133.
9. Crowe, W.E.; Goldberg, D.R. J. Am. Chem. Soc. 1995, 117, 5162. Crowe, W. E.; Goldberg, D. R.; Zhang, Z. J. Tetrahedron Lett. 1996, 37, 2117. Finkelshtein, E.Sh., Ushakov, N.V., Portnykh, E.B. J. Mol. Catalysis 1992, 76, 133.
10. For example, see: Yatagi, H.; Yamamoto, Y.; Maruyama, K. J. Am. Chem. Soc. 1980, 102, 4548. Yamamoto, Y. Acc. Chem. Res. 1987, 20, 243.
11. For example, see: Yatagi, H.; Yamamoto, Y.; Maruyama, K. J. Am. Chem. Soc. 1980, 102, 4548. Yamamoto, Y. Acc. Chem. Res. 1987, 20, 243.
12. For example, see: Keck, G.E.; Yates, J.B. J. Am. Chem. Soc. 1982, 104, 5829.
13. Ethylene wich is a stoichiometric cross metathesis byproduct resulting from cycloreversion steps has been omitted from the Scheme.
14. 1H-NMR spectrum. The identity of the major isomer was elucidated from the coupling constants of the olefinic hydrogens.
15. 2-Sn), 1.60-1.37 (m, 6H, Bu), 1.37-1.18 (m, 9H, Bu), 0.97-0.78 (m, 15H, Bu).
16. For examples for the synthesis of allyl silanes see: Brümmer, O.; Rückert, A.; Blechert, S. Chem. Eur. J., in press.