Synthesis and spectroscopic characterization of five-coordinate complexes of Ni2+ based on N3-macrocycles and salicylaldiminates. Crystal structure of [Ni(9-Me-N3-mc)(OC6H4CH=NC6H 5-o)](ClO4) (9-Me-N3-mc=2,4,4,9-tetramethyl-1,5,9-triazacyclododec-1-ene)

Inorganica Chimica Acta

Volumn 255, Issue 1, 1997, Pages 21-27

  Santana, M Dolores ^a   Rufete, Antonio ^a   Sánchez, Gregorio ^a   García, Gabriel ^a   López, Gregorio ^a   Casabó, Jaume ^b   Molins, Elíes ^c   Miravitlles, Carles ^c  

^a UNIVERSITY OF MURCIA   (Spain)

^b UNIVERSITAT AUTÒNOMA DE BARCELONA   (Spain)

^c INSTITUT DE CIÈNCIA DE MATERIALS DE BARCELONA ICMAB CSIC   (Spain)

Author keywords

Crystal structures; Macrocycle complexes; Nickel complexes; Pentacoordinate complexes

Indexed keywords

COORDINATION REACTIONS; CRYSTAL STRUCTURE; SYNTHESIS (CHEMICAL);

COORDINATE COMPLEXES; MACROCYCLE COMPLEX; NICKEL COMPLEX; PARAMAGNETIC SPECIES; PENTACOORDINATE COMPLEXES; PYRAMIDAL COORDINATION; SPECTROSCOPIC CHARACTERIZATION; X-RAY DIFFRACTION STUDIES;

NICKEL COMPOUNDS;

EID: 0002604288     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/s0020-1693(96)05199-7     Document Type: Article

References (25)

1. G. López, G. García, G. Sánchez, J. García, J. Ruiz, J.A. Hermoso, A. Vegas and M. Martínez-Ripoll, Inorg. Chem., 31 (1992) 1518.
2. G. López, G. Sánchez, G. García, J. García, A. Martínez, J.A. Hermoso and M. Martínez-Ripoll, J. Organomet. Chem., 435 (1992) 193.
3. G. López, G. Sánchez, G. García, J. García, A. Sanmartín and M.D. Santana, Polyhedron, 10 (1991) 2821.
4. G. Sánchez, J.A. Muñoz, M.J. Vidal, G. García and G. López, J. Organomet. Chem., 463 (1993) 239.
5. G. Sánchez, F. Momblona, G. García, G. López, E. Pinilla and A. Monge, J. Chem. Soc., Dalton Trans., (1994) 2271.
6. G. Sánchez, F. Ruiz, M.D. Santana, G. García, G. López, J.A. Hermoso and M. Martínez-Ripoll, J. Chem. Soc., Dalton Trans., (1994) 19.
7. G. López, G. Sánchez, G. García, J. Ruiz, J. García, M. Martínez-Ripoll, A. Vegas and J. A. Hermoso, Angew. Chem., Int. Ed. Engl., 30 (1991) 716.
8. J.W.L. Martin, J.H. Johnston and N.F. Curtis, J. Chem. Soc., Dalton Trans., (1978) 68.
9. L.J. Zompa, Inorg. Chem., 17 (1978) 2531.
10. R.W. Renfrew, R.S. Jamison and D.C. Weatherburn, Inorg. Chem., 18 (1979) 1584.
11. A. Escuer, R. Vicente and J. Ribas, Polyhedron, 11 (1992) 453.
12. C. Benelli, A. Dei, D. Gatteschi and L. Pardi, Inorg. Chem., 29 (1990) 3409.
13. G.C. Percy and D.A. Thornton, J. Inorg. Nucl. Chem., 34 (1972) 3357.
14. P. Main, G. Germain and M.M. Woolfson, MULTAN 11/80, a system of computer programs for the automatic solutions of crystal structures from X-ray diffraction data, Universities of York, UK, and Louvain, Belgium, 1980.
15. G.M. Sheldrick, SHELX 76, program for crystal structure determination, University of Cambridge, UK, 1976.
16. W.J. Geary, Coord. Chem. Rev., 7 (1971) 81.
17. C. Benelli, A. Dei, D. Gatteschi and L. Pardi, J. Am. Chem. Soc., 110 (1988) 6897.
18. J.E. Sarneski and C.N. Reilley, Inorg. Chem., 13 (1974) 977.
19. A. Dei and M. Wicholas, Inorg. Chim. Acta, 166 (1989) 151.
20. G.N. La Mar, W. Horrocks, Jr. and R.H. Holm (eds.), NMR of Paramagnetic Molecules, Academic Press, New York, 1973, p. 243.
21. J.D. Thwaites, I. Bertini and L. Sacconi, Inorg. Chem., 5 (1966) 1036.
22. S.D. Emerson, J.T.J. Lecomte and G.N. La Mar, J. Am. Chem. Soc., 110 (1988) 4176.
23. L. Banci, M. Piccioli and A. Scozzafaca, Coord. Chem. Rev., 120 (1992) 1, and Refs. therein.
24. J. Lisowski, L. Latos-Grazyñski and L. Szterenberg, Inorg. Chem., 31 (1992) 1933.
25. E.A. Lalancette and D.R. Eaton, J. Chem. Phys., 86 (1964) 5145.