Synthesis and characterization of the anionic fluorocarboranes 6,7,8,9,10-CB9H5F5-,6,7,8,9-CB 9H5F4-10-OH-, and 6,7,8,9-CB9H5F4-10-NHCOCH3 -

Inorganica Chimica Acta

Volumn 289, Issue 1-2, 1999, Pages 76-84

  Ivanov, Sergei V ^a,b   Ivanova, Svetlana M ^a   Miller, Susie M ^a   Anderson, Oren P ^a   Solntsev, Konstantin A ^b   Strauss, Steven H ^a  

^a Department of Environmental and Radiological Health Sciences   (United States)

^b KURNAKOV INSTITUTE OF GENERAL AND INORGANIC CHEMISTRY   (Russian Federation)

Author keywords

Carboranes; Fluorination

Indexed keywords

ACETONITRILE; DYES; FLUORINATION; ISOMERS; LIQUID CHROMATOGRAPHY; MIXTURES; NEGATIVE IONS; ORGANIC SOLVENTS; SALTS; TRIFLUOROACETIC ACID;

CARBORANES; CHROMATOGRAPHIC SEPARATIONS; CONCENTRATION RATIO; LEAST SQUARES REFINEMENT; REACTION MIXTURE; SPECTROSCOPIC CHARACTERIZATION; SYNTHESIS AND CHARACTERIZATIONS; TETRAFLUOROBORATES;

X RAY CRYSTALLOGRAPHY;

EID: 0002593742     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/s0020-1693(99)00060-2     Document Type: Article

References (46)

1. T. Jelínek, J. Plešek, S. Heřmánek, B. Štíbr, Coll. Czech. Chem. Commun. 51 (1986) 819.
2. Liston D.J., Lee Y.J., Scheidt W.R., Reed C.A. J. Am. Chem. Soc. 111:1989;6643.
3. Jelínek T., Baldwin P., Scheidt W.R., Reed C.A. Inorg. Chem. 32:1993;1982.
4. F.S. Mair, J.H. Morris, D.F. Gaines, D. Powell, J. Chem. Soc., Dalton Trans. (1993) 135.
5. Z. Xie, D. Liston, T. Jelínek, V. Mitro, R. Bau, C.A. Reed, J. Chem. Soc., Chem. Commun. (1993) 384.
6. Xie Z., Jelínek T., Bau R., Reed C.A. J. Am. Chem. Soc. 116:1994;1907.
7. Xie Z., Bau R., Reed C.A. Angew. Chem. Int. Ed. Engl. 33:1994;2433.
8. Xie Z., Bau R., Reed C.A. Inorg. Chem. 34:1995;5403.
9. Xie Z., Manning J., Reed R.W., Mathur R., Boyd P.D.W., Benesi A., Reed C.A. J. Am. Chem. Soc. 118:1996;2922.
10. Xie Z., Tsang C.-W., Xue F., Mak T.C.W. Inorg. Chem. 36:1997;2246.
11. Srivastava R.R., Hamlin D.K., Wilbur D.S. J. Org. Chem. 61:1996;9041.
12. Ivanov S.V., Lupinetti A.J., Miller S.M., Anderson O.P., Solntsev K.A., Strauss S.H. Inorg. Chem. 34:1995;6419.
13. Ivanov S.V., Ivanova S.M., Miller S.M., Anderson O.P., Solntsev K.A., Strauss S.H. Inorg. Chem. 35:1996;6914.
14. Ivanov S.V., Rockwell J.J., Miller S.M., Anderson O.P., Solntsev K.A., Strauss S.H. Inorg. Chem. 35:1996;7882.
15. Ivanov S.V., Rockwell J.J., Lupinetti A.J., Solntsev K.A., Strauss S.H. Siebert W. Advances in Boron Chemistry. 1997;430 Royal Society of Chemistry, Cambridge.
16. Ivanov S.V., Ivanova S.M., Miller S.M., Anderson O.P., Kuznetsov N.T., Solntsev K.A., Strauss S.H. Collect. Czech. Chem. Commun. 62:1997;1310.
17. Ivanov S.V., Rockwell J.J., Polyakov O.G., Gaudinski C.M., Anderson O.P., Solntsev K.A., Strauss S.H. J. Am. Chem. Soc. 129:1998;4224.
18. Ivanov S.V., Lupinetti A.J., Solntsev K.A., Strauss S.H. J. Fluorine Chem. 89:1998;65.
19. S.V. Ivanov, A.J. Lupinetti, S.M. Ivanova, S.M. Miller, O.P. Anderson, K.A. Solntsev, S.H. Strauss, manuscript in preparation.
20. S.V. Ivanov, J.J. Rockwell, F.M. Dixon, S.M. Miller, O.P. Anderson, K.A. Solntsev, S.H. Strauss, manuscript in preparation.
21. King B.T., Janousek Z., Gruner B., Trammell M., Noll B.C., Michl J. J. Am. Chem. Soc. 118:1996;3313.
22. J. Michl, B.T. King, I. Zharov, S. Moss, J. Clayton, J.T. Ceremuga, L. Pospisil, Abstract INOR-403, 215th ACS National Meeting, Dallas, TX (March/April 1998).
23. R. Dagani, Chem. Eng. News, May 4, 1998, p. 49.
24. Reed C.A. Accounts Chem. Res. 31:1998;325.
25. Strauss S.H. Chem. Rev. 93:1993;927.
26. Lupinetti A.J., Strauss S.H. Chemtracts Inorg. Chem. 11:1998;565.
27. Wiersema R.J., Hawthorne M.F. Inorg. Chem. 12:1973;785.
28. Shriver D.F., Drezdzon M.A. The Manipulation of Air-Sensitive Compounds. 2nd ed. 1986;Wiley-Interscience, New York.
29. Nestor K., Stíbr B., Kennedy J.D., Thornton-Pett M., Jelínek T. Coll. Czech. Chem. Commun. 57:1992;1262.
30. Hop C.E.C.A., Saulys D.A., Gaines D.F. Inorg. Chem. 34:1996;1977.
31. G.M. Sheldrick, SHELXTL, version 5.03, 1994.
32. G.M. Sheldrick, SHELXL-96, version 2(β), 1996.
33. Flack H.D. Acta Crystallogr., Sect. A. 39:1983;876.
34. Bernardinelli G., Flack H.D. Acta Crystallogr., Sect. A. 41:1985;500.
35. Thomsen H., Haeckel O., Krause U., Preetz W. Z. Anorg. Allg. Chem. 622:1996;2061.
36. Lal G.S., Pez G.P., Syvret R.G. Chem. Rev. 96:1996;1737.
37. Jung F., Tin K.C., Durst T. Int. J. Sulfur Chem. 8:1973;1.
38. Radhakrish-Namurti P.S., Sahu N.C. Indian J. Chem. 20A:1981;269.
39. R.E. Banks, M.K. Besheesh, S.N. Mohialdin-Khaffaf and I. Sharif, J. Chem. Soc., Perkin Trans. I (1996) 2069.
40. Dou D., Mavunkal I.J., Bauer J.A.K., Knobler C.B., Hawthorne M.F., Shore S.G. Inorg. Chem. 33:1994;6432.
41. T. Whelan, P. Brint, T.R. Spalding, W.S. McDonald, D.R. Lloyd, J. Chem. Soc., Perkin Trans. (1982) 2469.
42. F.H. Allen, O. Kennard, D.G. Watson, L. Brammer, A.G. Orpen, R. Taylor, J. Chem. Soc., Perkin Trans. II (1987) S1.
43. Andrieux C.P., Differding E., Robert M., Savéant J.-M. J. Am. Chem. Soc. 115:1993;6592.
44. Miller H.C., Hertler W.R., Muetterties E.L., Knoth W.H., Miller N.E. Inorg. Chem. 4:1965;1216.
45. Knoth W.H., Miller H.C., England D.C., Parshall G.W., Muetterties E.L. J. Am. Chem. Soc. 84:1962;1056.
46. Zupan M., Iskra J., Stavber S. Tetrahedron. 52:1996;11341.