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25844520283
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note
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3 TMS internal, 295 K; δ [ppm]: 141.45, 141.40, 141.05, 141.02, 138.90, 138.86, 138.60, 138.58, 138.40, 138.33, 136.61, 136.55, 130.04, 130.01, 129.04, 129.04, 127.23, 127.21, 126.70, 126.57, 126.39, 126.34, 119.62, 119.61, 119.56, 119.55, 21.76, 21.71.
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33
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25844526044
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note
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2O).
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34
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0010198266
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25844472025
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Ph.D. Thesis, The Hebrew University of Jerusalem, Jerusalem
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The preparation of 3 has previously been described: A. Ayalon, Ph.D. Thesis, The Hebrew University of Jerusalem, Jerusalem, 1993
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(1993)
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Ayalon, A.1
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38
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32544454854
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The MeOH capillary was calibrated against a standard MeOH sample supplied by Bruker Analytical Instruments and gave identical temperatures within ±1 K. For a calibration curve of the "methanol NMR thermometer" see A.L. van Geet, Anal.Chem., 1968, 40, 2227-2229
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41
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25844505632
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Z, are neglected
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Z, are neglected.
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