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0442270500
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note
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To a cooled solution of vinyl benzylamine (5 mmol) in 2 mL of methanol was added (R)-(+)-styrene epoxide (10 mmol) in 4 mL of methanol at 0°C and stirred for 1 h. It was then refluxed for 4 h. After completion of the reaction, the solvent was then removed under reduced pressure to give a syrupy mass which upon column chromatography (alumina) using ethyl acetate:hexane (10:90) as eluent gave the product (yield 30%).
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22
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0442302061
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note
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To 1 mol of (R,R)-3-aza-3-(p-vinylben/yl)-1,5-diphenyl-1,5-dihydroxypentane were added 1 mol of divinylbenzene and 4 mol of styrene in the presence of 10 mg of benzoyl peroxide, and it was sealed in a nitrogen atmosphere. Then the reaction mixture was heated at 70°C for 48 h.
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24
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0000726317
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0033522735
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31
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0442286113
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note
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4. Removal of the solvent under reduced pressure gave a syrupy mass, which upon flash column chromatography gave the product.
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32
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0025992275
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35
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0442302051
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note
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+ as the enolate, thus reducing the number of active chiral catalyst centers.
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