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26844506504
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note
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Furan derivative 6 was prepared from commercially available 3,4-bis(acetoxymethyl)furan by hydrolysis of the acetate and etherification of the diol with MOMCl.
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38
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0016414239
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41
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26844556770
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note
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4 reduction of the ketose gave the desired alcohol 17 together with an unidentified product which might be an overreduction product having a tetrahydropyran skeleton.
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42
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33845375399
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43
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26844541425
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note
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3) 20.68, 20.71, 20.87, 22.70, 60.62, 63.08, 63.57, 67.97, 70.76, 71.93, 76.58, 76.83, 78.24, 82.00, 86.70, 103.17, 127.86, 128.34, 128.67, 136.69, 168.99, 169.37, 169.57, 169.95.
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