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Tetrahedron Letters

Volumn 19, Issue 39, 1978, Pages 3657-3660

Mild methods for the in situ generation of trimethylsilyl iodide

(2) Jung, Michael E a Blumenkopf, Todd A a

a UNIVERSITY OF CALIFORNIA (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0002085932 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(01)95022-1 Document Type: Article

Times cited : (60)

References (24)

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8
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- Ho¹ Olah²

13
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16
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17
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- M. E. Jung and M. A. Lyster, Org. Syn., accepted for publication

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21
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- These authors report only a 32% yield of 7. Our 200 MHz NMR analysis indicated that 7 was a mixture of cis and trans isomers.
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24
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- Although the reaction vessel and solvents are carefully dried before using, there is always the possibility of adventitious water being present (and thus generating HI). There may be other reasons for the faster dealkylation with 4 but they have not yet been identified.

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