Titanocene(II)-promoted reaction of thioacetals with alkynes: Highly stereoselective preparation of conjugated dienes

Chemical Communications

Volumn , Issue 11, 1997, Pages 1055-1056

  Takeda, Takeshi ^a   Shimokawa, Hirohisa ^a   Miyachi, Yoshinaga ^a   Fujiwara, Tooru ^a  

^a TOKYO UNIVERSITY OF AGRICULTURE AND TECHNOLOGY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0002037964     PISSN: 13597345     EISSN: None     Source Type: Journal    
DOI: 10.1039/a701952a     Document Type: Article

References (18)

1. J. D. Meinhart and R. H. Grubbs, Bull. Chem. Soc. Jpn., 1988, 61, 171.
2. K. M. Doxsee and J. K. M. Mouser, Organometallic, 1990, 9, 3012.
3. K. M. Doxsee and J. K. M. Mouser, Tetrahedron Lett., 1991, 32, 1687.
4. N. A. Petasis and D.-K. Fu, Organometallies, 1993, 12, 3776 and references cited therein; K. M. Doxsee, J. J. J. Juliette, J. K. M. Mouser and R. Zientara, Organometallics, 1993, 12, 4682.
5. N. A. Petasis and D.-K. Fu, Organometallies, 1993, 12, 3776 and references cited therein; K. M. Doxsee, J. J. J. Juliette, J. K. M. Mouser and R. Zientara, Organometallics, 1993, 12, 4682.
6. For the preparation of trimethylsilyl- and methylene-titanacyclobutenes, see (a) N. A. Petasis, J. P. Staszewski and D.-K. Fu, Tetrahedron Lett., 1995, 36, 3619; (b) R. Beckhaus, K. H. Thiele and D. Ströhl, J. Organomet. Chem., 1989, 369, 43; (c) R. Beckhaus, J. Sang, T. Wagner and U. Englert, Organometallics, 1996, 15, 1176; (d) N. A. Petasis and Y.-H. Hu, J. Org. Chem., 1997, 62, 782.
7. For the preparation of trimethylsilyl- and methylene-titanacyclobutenes, see (a) N. A. Petasis, J. P. Staszewski and D.-K. Fu, Tetrahedron Lett., 1995, 36, 3619; (b) R. Beckhaus, K. H. Thiele and D. Ströhl, J. Organomet. Chem., 1989, 369, 43; (c) R. Beckhaus, J. Sang, T. Wagner and U. Englert, Organometallics, 1996, 15, 1176; (d) N. A. Petasis and Y.-H. Hu, J. Org. Chem., 1997, 62, 782.
8. For the preparation of trimethylsilyl- and methylene-titanacyclobutenes, see (a) N. A. Petasis, J. P. Staszewski and D.-K. Fu, Tetrahedron Lett., 1995, 36, 3619; (b) R. Beckhaus, K. H. Thiele and D. Ströhl, J. Organomet. Chem., 1989, 369, 43; (c) R. Beckhaus, J. Sang, T. Wagner and U. Englert, Organometallics, 1996, 15, 1176; (d) N. A. Petasis and Y.-H. Hu, J. Org. Chem., 1997, 62, 782.
9. For the preparation of trimethylsilyl- and methylene-titanacyclobutenes, see (a) N. A. Petasis, J. P. Staszewski and D.-K. Fu, Tetrahedron Lett., 1995, 36, 3619; (b) R. Beckhaus, K. H. Thiele and D. Ströhl, J. Organomet. Chem., 1989, 369, 43; (c) R. Beckhaus, J. Sang, T. Wagner and U. Englert, Organometallics, 1996, 15, 1176; (d) N. A. Petasis and Y.-H. Hu, J. Org. Chem., 1997, 62, 782.
10. Y. Horikawa, T. Nomura, M. Watanabe, I. Miura, T. Fujiwara and T. Takeda, Tetrahedron Lett., 1995, 36, 8835.
11. Y. Horikawa, M. Watanabe, T. Fujiwara and T. Takeda, J. Am. Chem. Soc., 1997, 119, 1127.
12. F. N. Tebbe and L. J. Guggenberger, J. Chem. Soc., Chem. Commun., 1973, 227; F. W. Hartner, Jr. and J. Schwartz, J. Am. Chem. Soc., 1981, 103, 4979.
13. F. N. Tebbe and L. J. Guggenberger, J. Chem. Soc., Chem. Commun., 1973, 227; F. W. Hartner, Jr. and J. Schwartz, J. Am. Chem. Soc., 1981, 103, 4979.
14. N. A. Petasis and E. I. Bzowej, J. Org. Chem., 1992, 57, 1327.
15. N. A. Petasis and I. Akritopoulou, Synlett, 1992, 665.
16. N. A. Petasis and E. I. Bzowej, Tetrahedron Lett., 1993, 34, 943.
17. R. Beckhaus, J. Oster and T. Wagner. Chem. Ber., 1994, 127, 1003.
18. J. X. McDermott, M. E. Wilson and G. M. Whitesides, J. Am. Chem. Soc., 1976, 98, 6529.