Monomeric N-lithioaryl- and N-lithioborylstannylamines from distannylamines

European Journal of Inorganic Chemistry

Volumn , Issue 9, 1998, Pages 1343-1349

  Seifert, Thomas ^a   Storch, Wolfgang ^a   Vosteen, Martina ^a  

^a UNIVERSITY OF MUNICH   (Germany)

Author keywords

Amides; Distannylamines; N lithioborylamines; N lithiostannylamines; Structure elucidation

Indexed keywords

AMIDES; ATOMS; LITHIUM; MAGNETIC RESONANCE SPECTROSCOPY; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE; TIN COMPOUNDS;

8-AMINOQUINOLINE; CLEAVAGE REACTION; DISTANNYLAMINE; MOLAR RATIO; MONOMERICS; MULTINUCLEAR MAGNETIC RESONANCE; N-LITHIOBORYLAMINE; N-LITHIOSTANNYLAMINE; NITROGEN ATOM; STRUCTURE ELUCIDATION;

NITROGEN;

EID: 0001940182     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/(sici)1099-0682(199809)1998:9<1343::aid-ejic1343>3.0.co;2-d     Document Type: Article

References (39)

1. [1a] W. Storch, H. Nöth, Angew. Chem. 1976, 88, 231; Angew. Chem. Int. Ed. Engl. 1976, 15, 235.
2. [1a] W. Storch, H. Nöth, Angew. Chem. 1976, 88, 231; Angew. Chem. Int. Ed. Engl. 1976, 15, 235.
3. [1b] S. Diemer, H. Nöth, W. Storch, Functionally Substituted Diborylamines, in preparation.
4. [1c] A. Appel, C. Kober, C. Neumann, H. Nöth, M. Schmidt, W. Storch, Chem. Ber. 1996, 129, 175-189 and refs. quoted therein.
5. D. R. Armstrong, D. Barr, R. Snaith, Angew. Chem. 1991, 103, 1702-1704; Angew. Chem. Int. Ed. Engl. 1991, 30, 1707-1709.
6. D. R. Armstrong, D. Barr, R. Snaith, Angew. Chem. 1991, 103, 1702-1704; Angew. Chem. Int. Ed. Engl. 1991, 30, 1707-1709.
7. [3a] B. Wrackmeyer, B. Schwarze, J. Weidinger, M. Milius, Z. Naturforsch. 1997, 52b, 431-433.
8. [3b] M. Westerhausen, W. Schwarz, Z. Anorg. Allg. Chem. 1993, 619, 1053-1063.
9. [3c] T. Fjeldberg, P. B. Hitchcock, M. F. Lappert, A. J. Thorne, J. Chem. Soc., Chem. Commun. 1984, 822-826.
10. [3d] R. Köster, G. Seidel, Angew. Chem. 1981, 93, 1009-1010; Angew. Chem. Int. Ed. Engl. 1981, 20, 972-973.
11. [3d] R. Köster, G. Seidel, Angew. Chem. 1981, 93, 1009-1010; Angew. Chem. Int. Ed. Engl. 1981, 20, 972-973.
12. [4a] K. Jones, M. F. Lappert, Proc. Chem. Soc. 1962, 358-359.
13. [4b] K. Jones, M. F. Lappert, J. Chem. Soc. 1965, 1944-1951.
14. B. Wrackmeyer, G. Kehr, H. Zhuo, S. Ali, Magn. Res. Chem. 1996, 34, 921-928.
15. W. Storch, H. Nöth, Chem. Ber. 1977, 110, 1636-1642.
16. G. Schmid, R. Boese, D. Bläser, Z. Naturforsch. 1982, B37, 1230-1236; H. Nôth, H. Prigge, A.-R. Rotsch, Chem. Ber. 1977, 119, 1361-1367.
17. G. Schmid, R. Boese, D. Bläser, Z. Naturforsch. 1982, B37, 1230-1236; H. Nôth, H. Prigge, A.-R. Rotsch, Chem. Ber. 1977, 119, 1361-1367.
18. S. Lustig, Diplomarbeit, Universität München, 1994.
19. B. Wrackmeyer, W. Storch, M. Vosteen, NMR Studies on Lithiostannylamines and -imines. in preparation.
20. H. Chen, R. A. Bartlett, M. M. Olmstead, P. P. Power, S. C. Shoner, J. Am. Chem. Soc. 1990, 112, 1048-1055.
21. C. Kober, J. Kroner, W. Storch, Angew. Chem. 1993, 105, 1693-1695; Angew. Chem. Int. Ed. Engl. 1993, 31, 1608-1610.
22. C. Kober, J. Kroner, W. Storch, Angew. Chem. 1993, 105, 1693-1695; Angew. Chem. Int. Ed. Engl. 1993, 31, 1608-1610.
23. R. Hulme, J. Chem. Soc. 1963, 1524-1527; V. G. Kumar Das, L. K. Mun, W. Chen, Organometallics, 1987, 6, 10-14.
24. R. Hulme, J. Chem. Soc. 1963, 1524-1527; V. G. Kumar Das, L. K. Mun, W. Chen, Organometallics, 1987, 6, 10-14.
25. C. Kober, H. Nöth, W. Storch, Chem. Ber. 1997, 130, 765-769.
26. C. Kober, H. Nöth, W. Storch, Structure Investigations of Distannazanes, in preparation.
27. S. Diemer, H. Nöth, K. Polborn, W. Storch, Chem. Ber. 1992, 125, 389-400.
28. W. Biffar, T. Gasparis-Ebeling, H. Nöth, W. Storch, B. Wrackmeyer, J. Magn. Res. 1981, 44, 54-61.
29. K. Gregory, P. V. R. Schleyer, R. Snaith, Adv. Inorg. Chem. 1991, 37, 47-49; R. E. Mulvey, Chem. Soc. Rev. 1991, 20, 167-172.
30. K. Gregory, P. V. R. Schleyer, R. Snaith, Adv. Inorg. Chem. 1991, 37, 47-49; R. E. Mulvey, Chem. Soc. Rev. 1991, 20, 167-172.
31. Calculated from the sum of the covalent radii by applying the Schomaker-Stevenson correction: A. F. Wells, Structural Inorganic Chemistry, 4th ed., Clarendon, Oxford University Press, 1979, p. 236.
32. [19a] P. Paetzold, C. Pelzer, R. Boese, Chem. Ber. 1988, 121, 51-59.
33. [19b] R. A. Bartlett, X. Feng, M. M. Olmstead, P. R. Power, K. J. Weese, J. Am. Chem. Soc. 1988, 109, 4851-4854.
34. SHELXTL-Plus, PC version, Siemens Analytical X-ray Instruments, Inc., Madison, WI, 1980.
35. G. M. Sheldrick, SHELXL-97, Program for the Refinement of Crystal Structures, University of Göttingen, 1997.
36. K. Sisido, S. Kozima, J. Org Chem. 1964, 29, 907-909.
37. P. Otto, Ph. D. Thesis, University of Munich, 1986.
38. H. C. Brown, S. U. Kularni, J. Organomet. Chem. 1979, 168, 281-286.
39. C. M. Wright, E. L. Muetterties, Inorg. Synth. 1976, 10, 137-139.