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3 to 100 mg of resin, allowing it to swell, and then collecting data for 30 000 transients on a Bruker AC250 NMR over 5 h (Larry Spangle, Lilly P. Chem. Dept).
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14
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85037495041
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note
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3CN) to 10% A/ 90% B over 7.5 min. Both 218λ and 254λ were monitored. Purity was determined at 218λ since absorption was much stronger at this wavelength.
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