Synthesis and structure of the (tetrahydroxy)oligosiloxane [(tBuO)3SiOSi(OH)2]2O

Journal of the Chemical Society, Dalton Transactions

Volumn , Issue 5, 2000, Pages 627-628

  Rulkcns, Ron ^a   Coles, Martyn P ^a   Don Tilley, T ^b  

^a UNIVERSITY OF CALIFORNIA   (United States)

^b LAWRENCE BERKELEY NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001820745     PISSN: 1470479X     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (41)

1. P. D. Lickiss, Adr. Inorg. Chcm., 1995, 42, 147.
2. F. J. Feher and T. A. Budzichowski, Polyhedron, 1995,14, 3239.
3. (a) R. Murugavel, A. Voigt, M. G. Walawalkar and H. W. Roesky, Chem, Rev.,1996, 96, 2205;
4. (b) R. Murueavel, V. Chandrasekhar and H. W. Roesky, Acc. Chem. Res., 1996,29,183.
5. (a) T. Takiguchi, J. Am. Client. Soc., 1959, 81, 2359;
6. (b) P. Jutzi, G. Strassburger, M. Schneider, H.-G. Stammler and B. Neumann, OrganomctaUics, 1996, 15, 2842;
7. N. Winkhofer, H. W. Roesky, M. Noltemeyer and W. T. Robinson, Augen: Client., Int. Ed. Engl., 1992, 31, 599;
8. S. S. Al-Juaid, N. H. Buttrus, R. I. Damja, Y. Derouiche, C. Eaborn, P. B. Hitchcock and P. D. Lickiss, J. Organoinel. Chem., 1989, 371, 287;
9. (e) R. Murugavel, V. Chandrasekhar, A. Voigt, H. W. Roesky, H.-G. Schmidt and M. Noltemeyer, Organometaliics, 1995, 14, 5298;
10. (f) N. Winkhofer, A. Voigt, H. Dorn, H. W. Roesky, A. Steiner, D. Stalke and A. Relier, Angeu: Chem., Int. Ed. Engl., 1994,33, 1352.
11. (a) J. F. Brown, L. H. Vogt and P. I. Prescott, J. Am. Chem. Soc., 1964, 86, 1120;
12. (b) K. Olsson, Ark. Kemi., 1958, 13, 367;
13. K. Olsson, K. Olsson and C. Grömvall, Ark. Kemi., 1961, 17, 529;
14. M. Unno, S. B. Alias, H. Saito and H. Matsumoto, Organometaliics, 1996,15,2413.
15. (a) J. F. Brown and L. H. Vogt, J. Am. Chem. Soc., 1965, 87, 4313;
16. (b) J. F. Brown and L. H. Vogt, J. Am. Chem. Soc., 1965, 87, 4317;
17. T. W. Hambley, T. Maschmeyer and A. F. Masters, Appl. Organomet. Chem., 1992,6, 253;
18. F. J. Feher, D. A. Newman and J. F. Walzer, J. Am. Chem. Soc., 1989, 111, 1741;
19. (e) F. J. Feher and D. A. Newman, J. Am. Chem. Soc., 1990,112, 1931;
20. (f) F. J. Feher, T. A. Budzichowski, R. L. Blanski, K. J. Weller and J. W. Ziller, Organometaliics, 1991, 10,2526.
21. R. Murugavel, P. Böttcher, A. Voigt, M. G. Walawalker, H. W. Roesky, E. Parisini, M. Teichert and M. Noltemeyer, Chem. Commun., 1996,2417.
22. F. J. Feher, J. J. Schwab, D. Soulivong and J. W. Ziller, Main Group Chem., 1997, 2, 123.
23. Y. Abe and I. Kijima, Bull. Chem. Soc. Jpn., 1969,42, 1118.
24. C. S. Miner, Jr., L. A. Bryan, R. P. Holysz and G. W. Pedlow, Jr., Iml. Eng. Chem., 1947,39, 1368.
25. (a) K. W. Terry and T. D. Tilley, Chem. Mater., 1991, 3, 1001;
26. (b) K. W. Terry, C. G. Luemair and T. D. Tilley, J. Am. Chem. Soc., 1997. 119, 9745;
27. K. W. Terry, P. K. Gantzel and T. D. Tilley, Chem. Mater., 1992, 4, 1290;
28. K. W. Terry, P. K. Gantzel and T. D. Tilley, Inorg. Chem., 1993, 32, 5402;
29. (e) K. W. Terry, C. G. Lugmair, P. K. Gantzel and T. D. Tilley, Chem. Mater., 1996,8,274;
30. (f) K. Su and T. D. Tilley, Chem. Mater., 1997, 9, 588;
31. (g) K. Su, T. D. Tilley and M. J. Sailor, J. Am. Chem. Soc., 1996, 118, 3459;
32. (f) K. W. Terry, K. Su, T. D. Tilley and A. L. Rheingold, Polyhedron, 1998, 17, 891;
33. R. Rulkens and T. D. Tilley, J. Am. Chem. Soc., 1998. 120, 9959;
34. (j) R- Rulkens, J. L. Male, K. W. Terry, B. Olthof, A. Khodakov, A. T. Bell, E. Iglesia and T. D. Tilley, Chem. Mater., 1999. 11, 2966;
35. (k) M. P. Coles, C. G. Lugmair, K. W. Terry and T. D. Tilley, Chem. Mater., 2000,12, 122.
36. C. J. Brinker and G. W. Scherer, Sol-Gel Science: The Physics and Chemistry of Sol-Gel Processing, Academic Press, Ine, San Diego, CA, 1990.
37. An optimized synthetic procedure for 4 (isolated yield: 70%) was subsequently developed using a lower initial reaction temperature (-60 °C) and NEt3 as the HCl-acceptor.
38. (a) M. Schrami-Marth, A. Wokaun, M. Pohl and H.-L. Krauss, J. Chem. Soc., Faraday Trans., 1991, 87, 2635;
39. (b) L. M. Kustov, Top. Catal J., 1997, 4, 131.
40. C. E. F. Rickard, W. R. Roper, D. M. Salter and L. J. Wright, J. Am. Chem. Soc., 1992,114,9682.
41. P. D. Lickiss, S. A. Litser, A. D. Redhouse and C. J. Wisener, J. Chcm. Soc., Chem. Commun., 1991, 173.