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Crystallographic data (excluding structure factors) for the structures of 1, 1-thf, 2, and 4 have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-101239. Copies of the data can be obtained on application to CCDC, 12 Union Road, Cambridge, CB2 1EZ, U.K. [Fax: (internat.) + 44(0)1223/336033; E-mail: deposit@ccdc.cam.ac.uk].
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