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Tetrahedron Letters
Volumn 29, Issue 16, 1988, Pages 1927-1930
Allylic amination of alkenes by tosyliminoiodobenzene: manganese porphyrins as suitable catalysts
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EID: 0001743473     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(00)82081-X     Document Type: Article
Times cited : (143)
References (13)
  • 3
    • 84918471362 scopus 로고    scopus 로고
    • Mahy, J.P.; Bedi, G.; Battioni, P.; Mansuy, D., J. Chem. Soc., Perkin Trans II, in press.
  • 4
    • 84918471361 scopus 로고    scopus 로고
    • TDCPP and TPP stand respectively for the dianions of meso-tetra-orthodichlorophenylporphyrin and meso-tetraphenylporphyrin.
  • 5
    • 84918471360 scopus 로고    scopus 로고
    • 4.
  • 7
    • 84918471359 scopus 로고    scopus 로고
    • 4Si)) characteristics of the allylic N-tosylamines.3: m/z-91(100%); 155(50%); 224(82%); 253(1%); δ=0.82(t,3H, J=7.5Hz); 1–1.5(m,2H); 1.92(d,3H,J=7.5Hz); 2.40(s,3H); 3.58(m, 1H); 4.35(d, 1H,J=9.5Hz); 5.04(m, 1H); 5.35(m, 1H); 7.28(d,2H,J=7.5Hz); 7.72(d,2H,J=7.5Hz);4: m/z=91(100%); 155(25%); 238(22%); 253(1%); δ=0.82(t,3H, J=7.5Hz); 1–1.5(m,2H); 1.92(dt,2H); 2.40(s,3H); 3.86(m,1H); 4.31(d, 1H,J=9.5Hz); 5.13(m, 1H); 5.42(m, 1H); 7.28(d,2H,J=7.5Hz); 7.70(d,2H,J=7.5Hz).5: m/z=91(100%); 98(44%); 155(33%); 184(10%): 210(8%); 224 (10%); 253(3%); δ=0.82(t,3H,J=7.5Hz); 1–1.08(m,2H); 1.92(dt, 2H); 2.40(s,3H); 3.5(dd, 1H); 4.24(t, 1H,J=1OHz); 5.00(dd, 1H); 5.30(dt, 1H); 7.31(d,2H,J=7.5Hz); 7.72(d,2H,J=7.5Hz). Because of its low yields, 6 was only identified by G.C-mass spectrometry (m/z=91(100%); 155(68%); 210(75%) 253(1%)) [[Truncated]]

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