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C, H, N, S analyses were carried out by Atlantic Microlab, Inc., Norcross, GA
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C, H, N, S analyses were carried out by Atlantic Microlab, Inc., Norcross, GA.
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note
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Before this reaction, sulfonic acid-MCM-41 was washed with distilled water until the washings were neutral, followed by additional washing. The sample was then dried overnight under vacuum at 120 °C. No remaining nitrogen (e.g., due to nitric acid) was detected by chemical analysis.
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